Biogenic Fabrication of ZnO Nanoparticles Using Selenicereus undatus Peel Extract: Transforming Agricultural Residues into Value-Added Materials DOI Open Access

S Ruby,

Fr. John

Oriental Journal Of Chemistry, Journal Year: 2025, Volume and Issue: 41(2), P. 573 - 583

Published: April 28, 2025

This research delineates an innovative, eco-conscious synthesis method for zinc oxide nanomaterials utilizing Selenicereus undatus peel extract, underscoring the principles of green chemistry and transforming agricultural waste into a functional nanomaterial. Extensive optimization was carried out by varying precursor concentration, extract- ratio, pH, temperature reaction time. The ideal conditions—1:2 extract to 0.01M acetate, pH 9, 70°C, 3-hrs incubation—produced ZnO nanoparticles (SU-ZnO NPs) with high crystallinity. X-ray diffraction (XRD) confirmed hexagonal wurtzite phase average crystallite size 24.95 nm. Fourier transform infrared (FTIR) identified Zn–O bond formation at 538 cm⁻¹, while UV–diffuse reflectance spectroscopy (UV-DRS) indicated direct band gap energy 3.16 eV, suggesting potential optoelectronic applications. Field emission scanning electron microscopy (FE-SEM) showed well-defined nanorods (~98.16 nm) interconnected structure, enhancing mechanical stability conductivity. Energy-dispersive (EDS) analysis elemental composition, showing strong signals oxygen, verifying purity NPs. High-resolution transmission (HR-TEM) further these lattice fringes 0.26 nm, corresponding (002) plane, selected area (SAED) pattern matching ZnO’s crystallographic planes. Additionally, dynamic light scattering (DLS) zeta measurements highlighted colloidal uniform distribution nanoparticles. These findings underscore efficacy in nanotechnology, promoting sustainable, cost-effective alternatives NPs fabrication applications biomedical, environmental, electronic sectors.

Language: Английский

Dynamic Light Scattering and Its Application to Control Nanoparticle Aggregation in Colloidal Systems: A Review DOI Creative Commons

Jesus Rodriguez-Loya,

Maricarmen Lerma,

Jorge L. Gardea‐Torresdey

et al.

Micromachines, Journal Year: 2023, Volume and Issue: 15(1), P. 24 - 24

Published: Dec. 22, 2023

Colloidal systems and their control play an essential role in daily human activities, but several drawbacks lead to avoidance of extensive application some more productive areas. Some roadblocks are a lack knowledge regarding how influence address colloidal forces, as well practical devices understand these systems. This review focuses on applying dynamic light scattering (DLS) powerful tool for monitoring characterizing nanoparticle aggregation dynamics. We started by outlining the core ideas behind DLS it may be used examine particle size distribution dynamics; then, last section, we included options chemically processed toner. In addition, pinpointed gaps difficulties that obstruct use real-world situations. Although widely used, has limits when dealing with complicated systems, including combinations nanoparticles, high concentrations, non-spherical particles. discussed issues offered possible solutions incorporation supplementary characterization approaches. Finally, emphasized critical is close gap between fundamental studies translation into applications, recognizing challenges science.

Language: Английский

Citations

46

Antibacterial and Antibiofilm Activity of Green-Synthesized Zinc Oxide Nanoparticles Against Multidrug-Resistant Escherichia coli Isolated from Retail Fish DOI Creative Commons
Mohamed Tharwat Elabbasy, Rasha M. El Bayomi, Esraa A. Abdelkarim

et al.

Molecules, Journal Year: 2025, Volume and Issue: 30(4), P. 768 - 768

Published: Feb. 7, 2025

Multidrug-resistant (MDR) Escherichia coli is a major foodborne pathogen posing critical threat to public health, particularly through the contamination of animal products. The increasing prevalence and virulence MDR E. strains underscore urgent need for alternative antimicrobial strategies. This study aimed synthesize characterize zinc oxide nanoparticles (ZnO-NPs) using Stevia rebaudiana as sustainable capping reducing agent, aligning with green chemistry principles. Of 120 fish samples, 74.2% (89/120) were positive contamination. Among identified strains, 77.8% (119/153) classified MDR. Resistance profiling revealed 22 distinct patterns, seven highly resistant virulent selected further analyses. eco-friendly auto-combustion synthesis ZnO-NPs produced semi-spherical hexagonal shapes an average size ranging from 12 25 nm. Scanning Electron Microscope-Energy Dispersive X-ray analysis (SEM-EDS) confirms that primarily consist (37.5%) oxygen (19.9%), carbon (42.6%) indicating process. demonstrated potent, dose-dependent antibacterial antibiofilm activity against strains. Additionally, mechanistic studies disrupt bacterial cell membranes, alter cellular morphology, interfere DNA integrity. These findings highlight potential promising nanomaterial enhancing food safety addressing growing challenge bacteria.

Language: Английский

Citations

3

A Mechanistic Overview on Green Assisted Formulation of Nanocomposites and Their Multifunctional Role in Biomedical Applications DOI Creative Commons

Mahnoor Mahnoor,

Khafsa Malik, Abeer Kazmi

et al.

Heliyon, Journal Year: 2025, Volume and Issue: 11(3), P. e41654 - e41654

Published: Jan. 8, 2025

The importance of nanocomposites constantly attains attention because their unique properties all across the fields especially in medical perspectives. study green-synthesized has grown to be extremely fascinating field research. Nanocomposites are more promising than mono-metallic nanoparticles they exhibit synergistic effects. This review encapsulates current development formulation plant-mediated by using several plant species and impact secondary metabolites on biocompatible functioning. Phyto-synthesis produces diverse nanomaterials with biocompatibility, environment-friendliness, vivo actions, characterized varying sizes, shapes, biochemical nature. process is advantageous conventional physical chemical procedures. New studies have been conducted determine biomedical efficacy against various diseases. Unfortunately, there inadequate investigation into green-assisted nanocomposites. Incorporating phytosynthesized therapeutic interventions not only enhances healing processes but also augments host's immune defenses infections. highlights phytosynthesis applications, including antibacterial, antidiabetic, antiviral, antioxidant, antifungal, anti-cancer, other as well toxicity. explores mechanistic action achieve designated tasks. Biogenic for multimodal imaging potential exchange methods materials Well-designed utilized innovative theranostic agents subsequent objective efficiently diagnosing treating a variety human disorders.

Language: Английский

Citations

2

Cell Membrane‐Coated Nanoparticles: A New Frontier in Immunomodulation DOI Creative Commons
Nimeet Desai, Vishakha Tambe, Prasad Pofali

et al.

Advanced NanoBiomed Research, Journal Year: 2024, Volume and Issue: 4(8)

Published: May 31, 2024

Immune dysregulation is a pivotal factor in the onset and progression of various diseases. In cancer, immune system's inability to discern eliminate abnormal cells leads uncontrolled tumor growth. When faced with resilient pathogens or harmful toxins, system encounters challenges clearance neutralization. Achieving delicate balance pro‐inflammatory anti‐inflammatory signals essential managing range disorders Like other biomedical research domains, nanotechnology has provided innovative approaches for rebalancing host immunity. Among plethora nanotechnology‐based interventions, concept cell membrane‐coated nanoparticles holds significant potential immunomodulatory applications owing their biomimetic properties that allow precise interaction compromised system. This review thoroughly examines novel nanosystems modulation. The exploration covers crucial elements, including origins characteristics membranes, methods employed procurement coating, physicochemical/biological characterization techniques, enhancement therapeutic efficacy via functionalization. Subsequently, case studies‐based analysis utilizing these bioinspired tackling different conditions caused by disturbance been comprehensively discussed.

Language: Английский

Citations

12

Dynamic Light Scattering for the Measurement of Transport Properties of Fluids DOI Creative Commons
Thomas M. Koller, Michael H. Rausch, Andreas P. Fröba

et al.

International Journal of Thermophysics, Journal Year: 2024, Volume and Issue: 45(4)

Published: March 11, 2024

Abstract The present article summarizes experimental and theoretical considerations required for a proper use of dynamic light scattering (DLS) the measurement transport properties fluids. It addresses not only recent advancements method, but also aims to provide recommendations researchers who intend apply technique in future. As outlined this study, DLS is based on analysis scattered governed by microscopic statistical or periodic fluctuations that originate from thermal movement molecules and/or particles at macroscopic thermodynamic equilibrium. dynamics these hydrodynamic bulk fluids their phase boundaries are related underlying diffusive processes and, thus, associated properties, reflected time-dependent correlation function intensity. fundamentals type detection, known as photon spectroscopy (PCS), will be discussed contribution some more detail. emphasized experiments need designed carefully accordance with theory order assign signals corresponding fluctuations. If necessary conditions fulfilled, allows accurate determination several including kinematic viscosity, diffusivity, mutual sound attenuation, which may accessed together other thermophysical such speed surface interfacial tension. In instances, simultaneous possible. With exception expanded uncertainties mentioned down 1 % can achieved various types fluid systems over wide range states up elevated temperatures pressures well vicinity critical points. This performance versatility documented study highlighting examples property research different classes working relevant process energy technology.

Language: Английский

Citations

11

Chitosan/aloe vera gel coatings infused with orange peel essential oils for fruits preservation DOI Creative Commons

Wen Xia Ling Felicia,

Kobun Rovina,

Nasir Md Nur ‘Aqilah

et al.

Current Research in Food Science, Journal Year: 2024, Volume and Issue: 8, P. 100680 - 100680

Published: Jan. 1, 2024

Continuous fruit waste poses significant environmental and economic challenges, necessitating innovative coating technologies. This research focuses on harnessing discarded orange peels to extract essential oil (OPEO), which is then integrated into a chitosan/aloe vera (CTS/AVG) matrix. The study comprehensively characterised the in terms of its physicochemical properties, antioxidant capacity, antimicrobial efficacy. investigation involved an analysis particle size distribution solutions, highlighting changes induced by incorporation peel (1 %, 2 % 3 v/w) (4:1 v/v) matrix, including reduction enhanced Brownian motion. quantifies 33.21 decrease water vapour transmission rate diffusion coefficient from 9.26 × 10-11 m

Language: Английский

Citations

10

Green synthesis of magnesium oxide nanoparticles using endophytic fungal strain to improve the growth, metabolic activities, yield traits, and phenolic compounds content of Nigella sativa L. DOI Creative Commons

Mohamed A. Amin,

Abdelghafar M. Abu-Elsaoud, Abdelatti I. Nowwar

et al.

Green Processing and Synthesis, Journal Year: 2024, Volume and Issue: 13(1)

Published: Jan. 1, 2024

Abstract Endophytic fungus Penicillium crustosum EP-1 was used to create spherical shape magnesium oxide nanoparticles (MgO-NPs). The MgO-NPs possess a crystalline structure with sizes of 8–35 nm. weight percentages Mg and O were 42.44% 30.13%, respectively, as shown in energy-dispersive X-ray analysis. In addition, analysis involving dynamic light scattering indicated the uniformity within colloidal solution. These NPs displayed polydispersity index 0.341 held surface charge −29.7 mV. A field experimental carried out assess outcome foliar spraying at 5, 10, 20 ppm on growth, yield, metabolic activities Nigella sativa L. Our results that significantly enhanced various growth parameters, including chlorophyll content (both b), total carotenoids, carbohydrate protein levels both shoots seeds, well free proline concentration, compared control plants 55 75 days after planting. all yield traits markedly increased. Moreover, high-performance liquid chromatography is employed for identification phenolic compounds seeds. Data sex acids, two phenols, five flavonoids present high concentrations due treatment opposed untreated plants.

Language: Английский

Citations

10

Hyaluronic Acid – Coated Niosomes for Curcumin Targeted Delivery into Breast Cancer Cells DOI

Zahraa M. Al Zubaidi,

Hamdi Nsairat, Naeem Shalan

et al.

ChemistrySelect, Journal Year: 2024, Volume and Issue: 9(3)

Published: Jan. 17, 2024

Abstract This study described a hyaluronic acid (HA) coated niosomes (Nio) encapsulated curcumin (CRM) (CRM‐HA‐Nio) to improve therapeutic properties via targeted delivery. CRM‐HA‐Nio was prepared by thin film hydration method and characterized dynamic light scattering transmission electron microscopy. Release assay performed utilizing dialysis method. Antioxidant, Cell viability, cellular uptake assays were evaluate the biological activity. has 142.93±39.71 nm size with −20.67±1.10 charge showed good stability 93±4.35 % encapsulation efficiency displayed pH‐independent release pattern. 2‐fold antioxidant improvement compared free CRM. much better cytotoxic activity on MCF‐7 cell line IC 50 of 1.851±0.45 μM CRM equal 5.230±0.85 μM, approximately 3‐fold enhancement. may be promising nanocarrier elucidate bioactivity against cancer when oxidative stress is major side effect.

Language: Английский

Citations

9

Advances in the Optimization of Fe Nanoparticles: Unlocking Antifungal Properties for Biomedical Applications DOI Creative Commons

Zeshan Ali Sandhu,

Muhammad Asam Raza, Abdulmajeed Alqurashi

et al.

Pharmaceutics, Journal Year: 2024, Volume and Issue: 16(5), P. 645 - 645

Published: May 10, 2024

In recent years, nanotechnology has achieved a remarkable status in shaping the future of biological applications, especially combating fungal diseases. Owing to excellence nanotechnology, iron nanoparticles (Fe NPs) have gained enormous attention years. this review, we provided comprehensive overview Fe NPs covering key synthesis approaches and underlying working principles, factors that influence their properties, essential characterization techniques, optimization antifungal potential. addition, diverse kinds NP delivery platforms command highly effective release, with fewer toxic effects on patients, are great significance medical field. The issues biocompatibility, toxicity profiles, applications optimized field biomedicine also been described because these most significant determining inclusion clinical use. Besides this, difficulties regulations exist transition from laboratory experimental studies (toxicity, specific standards, safety concerns) NPs-based agents summarized.

Language: Английский

Citations

7

Biological Synthesis of Cerium Oxide Nanoparticles Using Funnel Extract: Characterization and Evaluation of Its Angiogenesis and Cytotoxicity Properties Against Breast Cancer Cells DOI

Salem Jabr Seyyed Al Khafaji,

Maryam Ghobeh,

Mohammad Mashergi

et al.

BioNanoScience, Journal Year: 2024, Volume and Issue: 14(5), P. 4825 - 4836

Published: March 12, 2024

Language: Английский

Citations

6