Optimization of a Pressurized Extraction Process Based on a Ternary Solvent System for the Recovery of Neuroprotective Compounds from Eucalyptus marginata Leaves DOI Open Access
Soumaya Hasni, Hajer Riguene, J. A. Mendiola

et al.

International Journal of Molecular Sciences, Journal Year: 2024, Volume and Issue: 26(1), P. 94 - 94

Published: Dec. 26, 2024

Green chemistry focuses on reducing the environmental impacts of chemicals through sustainable practices. Traditional methods for extracting bioactive compounds from Eucalyptus marginata leaves, such as hydro-distillation and organic solvent extraction, have limitations, including long extraction times, high energy consumption, potential toxic residues. This study explored use supercritical fluid (SFE), pressurized liquid (PLE), gas-expanded (GXL) processes to improve efficiency selectivity. These techniques were combined in a single mixture design, where CO2 was used experiments carried out under SFE, while water ethanol PLE GXL by varying concentration solvents cover all possibilities. The neuroprotective activity extracts evaluated measuring their antioxidant, anti-inflammatory, acetylcholinesterase inhibition properties. optimization resulted novel with an optimal ternary 27% CO2, 55% ethanol, 18% water, degree desirability (R2 = 88.59%). Chromatographic analysis GC-MS HPLC-ESI-MS/MS identified over 49 metabolites. designed process offers promising approach producing phenolic-rich plant industrial applications.

Language: Английский

Prospecting Pharmacologically Active Biocompounds from the Amazon Rainforest: In Vitro Approaches, Mechanisms of Action Based on Chemical Structure, and Perspectives on Human Therapeutic Use DOI Creative Commons
Andryo Orfi Almada-Vilhena, Oscar Vinícius Moraes dos Santos, Milla de Andrade Machado

et al.

Pharmaceuticals, Journal Year: 2024, Volume and Issue: 17(11), P. 1449 - 1449

Published: Oct. 30, 2024

The Amazon rainforest is an important reservoir of biodiversity, offering vast potential for the discovery new bioactive compounds from plants. In vitro studies allow investigation biological processes and interventions in a controlled manner, making them fundamental pharmacological biotechnological research. These approaches are faster less costly than vivo studies, providing standardized conditions that enhance reproducibility precision data. However, methods have limitations, including inability to fully replicate complexity living organism absence complete physiological context. Translating results models not always straightforward, due differences pharmacokinetics interactions. this context, aim literature review assess advantages disadvantages search drugs Amazon, identifying challenges limitations associated with these comparing testing. Thus, bioprospecting involves evaluating plant extracts through bioassays investigate pharmacological, antimicrobial, anticancer activities. Phenolic terpenes frequently identified as main agents, exhibiting antioxidant, anti-inflammatory, antineoplastic Chemical characterization, molecular modifications, development delivery systems, such nanoparticles, highlighted improve therapeutic efficacy. Therefore, offers great drugs; however, significant challenges, standardization extraction need clinical trials, must be overcome become viable medications.

Language: Английский

Citations

1

Optimization of a Pressurized Extraction Process Based on a Ternary Solvent System for the Recovery of Neuroprotective Compounds from Eucalyptus marginata Leaves DOI Open Access
Soumaya Hasni, Hajer Riguene, J. A. Mendiola

et al.

International Journal of Molecular Sciences, Journal Year: 2024, Volume and Issue: 26(1), P. 94 - 94

Published: Dec. 26, 2024

Green chemistry focuses on reducing the environmental impacts of chemicals through sustainable practices. Traditional methods for extracting bioactive compounds from Eucalyptus marginata leaves, such as hydro-distillation and organic solvent extraction, have limitations, including long extraction times, high energy consumption, potential toxic residues. This study explored use supercritical fluid (SFE), pressurized liquid (PLE), gas-expanded (GXL) processes to improve efficiency selectivity. These techniques were combined in a single mixture design, where CO2 was used experiments carried out under SFE, while water ethanol PLE GXL by varying concentration solvents cover all possibilities. The neuroprotective activity extracts evaluated measuring their antioxidant, anti-inflammatory, acetylcholinesterase inhibition properties. optimization resulted novel with an optimal ternary 27% CO2, 55% ethanol, 18% water, degree desirability (R2 = 88.59%). Chromatographic analysis GC-MS HPLC-ESI-MS/MS identified over 49 metabolites. designed process offers promising approach producing phenolic-rich plant industrial applications.

Language: Английский

Citations

0