Green sorbent-based microextraction techniques in sample preparation for food analysis DOI
Natalia Casado, Jorge A. M. Pereira, Sonia Morante‐Zarcero

et al.

Comprehensive analytical chemistry, Journal Year: 2023, Volume and Issue: unknown

Published: Jan. 1, 2023

Language: Английский

Consumer Trends in the Herbal Tea Market: A Systematic Literature Review DOI Creative Commons
Roberto Carbone, Francesco Caracciolo, Giuseppe Di Vita

et al.

Food Reviews International, Journal Year: 2025, Volume and Issue: unknown, P. 1 - 19

Published: April 16, 2025

Language: Английский

Citations

1
Recent food alerts and analytical advances related to the contamination of tropane and pyrrolizidine alkaloids in food DOI Creative Commons
Natalia Casado, Judith Gañán, Sonia Morante‐Zarcero

et al.

Frontiers in Chemical Biology, Journal Year: 2024, Volume and Issue: 3

Published: April 10, 2024

The food control of tropane and pyrrolizidine alkaloids has become in recent years Europe one the main priorities within safety field due to exponential increase alerts related concerning levels these natural toxins foods. This awareness led increasing progress research determination compounds. Hence, this mini-review provides a brief comprehensive overview evolution alerts, highlighting products frequently contaminated with reviewing analytical advances their las 3 (from 2020 2023).

Language: Английский

Citations

4
Advances in Greener and Sustainable Sample Preparation for Tropane Alkaloid Analysis in Foods DOI
Lorena González-Gómez, Begoña Fernández-Pintor, Judith Gañán

et al.

Springer eBooks, Journal Year: 2025, Volume and Issue: unknown, P. 1 - 31

Published: Jan. 1, 2025

Language: Английский

Citations

0
Chiral HPLC-MS/MS determination of hyoscyamine enantiomers in baby herbal infusions after preconcentration with sulfonic HMS mesostructured silica synthesized by co-condensation DOI Creative Commons
Fernando L. Vera-Baquero, Judith Gañán, Sonia Morante‐Zarcero

et al.

Microchemical Journal, Journal Year: 2024, Volume and Issue: 198, P. 110150 - 110150

Published: Feb. 13, 2024

Tropane alkaloids are considered a major food safety issue in recent years, due to their worrying appearance many foods, such as herbal infusions, usually cross-contamination with weeds during harvest. (−)-Hyoscyamine is synthesized by tropane alkaloids-producing plants and its ingestion can cause all types of disorders humans. Its enantiomerization occurs easily over time, so the inactive (+)-hyoscyamine be found foods variable proportions. Therefore, goal current work was develop chiral high performance liquid chromatography tandem mass spectrometry method for enantiomeric determination (−)- (+)-hyoscyamine. Chromatographic separation optimized, best resolution (Rs = 1.59) achieved 6.5 min Chiralpak® AY-3 polysaccharide-based stationary phase column using ethanol 0.05 % diethylamine mobile phase. For preconcentration sample, two mesostructured silicas sulfonic groups were synthesized, grafting co-condensation methods, characterized. The materials evaluated sorbents strong-cation exchange solid-phase extraction hyoscyamine baby infusions. Based on findings gathered, silica denoted HMS-SO3−(co) sorbent number functional attached (2.63 mmol/g) textural properties. Under optimal conditions, factor obtained 167, only 50 mg material, very low racemization (−)-hyoscyamine (+) enantiomer (<20 %). validated recoveries 94–99 %, good linearity (R2 > 0.99), precision (RSD < 20 %), no matrix effect both analytes quantification limit (0.089 µg/L 0.092 (−)-hyoscyamine, respectively) meet applicability monitoring real samples. Two teas babies (instant tea bags) analyzed developed methodology. instantaneous infusions analysed contaminated, one them 0.21 0.09 (ratio 70(−)/30(+)) other 0.075 (the (+)- below method). Taking these results into account, it important evaluate content enantiomers avoid overestimation exposure.

Language: Английский

Citations

3
Detection of tropane alkaloid contaminations in unprocessed soybeans and their fate in food and feed processing DOI Creative Commons
Bernhard Blank‐Landeshammer,

Christa Ranetbauer,

Julian Weghuber

et al.

Food Control, Journal Year: 2024, Volume and Issue: unknown, P. 110963 - 110963

Published: Oct. 1, 2024

Language: Английский

Citations

1
Lapachol, a natural food component, interacts with human serum albumin: Insights of its impact on the pharmacokinetics of clinically used drugs DOI
Zaida L. Almeida, Pedro F. Cruz, Telma Costa

et al.

International Journal of Biological Macromolecules, Journal Year: 2024, Volume and Issue: 282, P. 137520 - 137520

Published: Nov. 10, 2024

Language: Английский

Citations

1
Green sorbent-based microextraction techniques in sample preparation for food analysis DOI
Natalia Casado, Jorge A. M. Pereira, Sonia Morante‐Zarcero

et al.

Comprehensive analytical chemistry, Journal Year: 2023, Volume and Issue: unknown

Published: Jan. 1, 2023

Language: Английский

Citations

0