Sealing of cerium oxide coating primers on anodized AA2024-T3 alloy by boiling in Lourier buffers DOI Creative Commons
S. Kozhukharov, Christian Girginov, Stefania Portolesi

et al.

Journal of Electrochemical Science and Engineering, Journal Year: 2024, Volume and Issue: unknown

Published: Aug. 4, 2024

Although their exceptional re-passivation ability, Al-alloys are susceptible to corrosion due the amphoteric nature of alumina passivation films. This issue is exacerbated by disruption these films intermetallics on surfaces highly doped ones, like AA2024-T3 aircraft alloy. The combination anodized aluminium oxide (AAO) and cerium conversion coatings (CeCC) shows promise as a coating primer. However, defective structures CeO2 Al2O3 require additional sealing. research proposes sealing CeCC/AAO layer boiling it for 10 minutes in two relatively neutral Lourier buffers, adjusted pH 7.75, mixture them. samples underwent series analyses compare impact procedure surface topology, properties (e.g., colour wettability from each set), protective ability. It was assessed after 24 hours exposure 3.5 % NaCl model corrosive medium six set. assessments included electrochemical impedance spectroscopy (EIS) potentiodynamic scanning (PDS) techniques. results indicate that borate buffer improves protection primers more effectively than phosphate mixed ones.

Language: Английский

Mechanical Properties and Corrosion Resistance of Thin Ceria and Phosphate Mono- and Multilayers Deposited on Technically Pure Al 1050 DOI Open Access
Sabina Cherneva, Reni Andreeva, D. Stoychev

et al.

Materials, Journal Year: 2025, Volume and Issue: 18(2), P. 424 - 424

Published: Jan. 17, 2025

Calcium phosphates are often used for biomedical applications. Hydroxyapatite, example, has a wide range of applications because it mimics the mineral component natural bone. Widespread interest in catalytic properties ceria is due to its use automotive converters. Effect electroless deposited on (non-anodized and anodized) Al 1050 with monolayer Ce2O3 + CeO2, consecutive bilayer CeO2/Ca5(PO4)3OH or CeO2/(AlPO4 AlOOH CePO4) systems indentation modulus (EIT) hardness (HIT), as well their corrosion-protective ability were investigated. For structural, chemical, electrochemical, mechanical characterization investigated systems, following methods used: scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDXS), photoelectron spectroscopy (XPS), polarization resistance (Rp), corrosion rate (CR) analysis, nanoindentation. It was found that HIT EIT coatings an anodized aluminum substrate much higher than those non-anodized substrate. established specific influence morphology chemical composition formed conversion layers improved effect these layers. The obtained results valuable since there no data such literature date.

Language: Английский

Citations

0

Sealing of cerium oxide coating primers on anodized AA2024-T3 alloy by boiling in Lourier buffers DOI Creative Commons
S. Kozhukharov, Christian Girginov, Stefania Portolesi

et al.

Journal of Electrochemical Science and Engineering, Journal Year: 2024, Volume and Issue: unknown

Published: Aug. 4, 2024

Although their exceptional re-passivation ability, Al-alloys are susceptible to corrosion due the amphoteric nature of alumina passivation films. This issue is exacerbated by disruption these films intermetallics on surfaces highly doped ones, like AA2024-T3 aircraft alloy. The combination anodized aluminium oxide (AAO) and cerium conversion coatings (CeCC) shows promise as a coating primer. However, defective structures CeO2 Al2O3 require additional sealing. research proposes sealing CeCC/AAO layer boiling it for 10 minutes in two relatively neutral Lourier buffers, adjusted pH 7.75, mixture them. samples underwent series analyses compare impact procedure surface topology, properties (e.g., colour wettability from each set), protective ability. It was assessed after 24 hours exposure 3.5 % NaCl model corrosive medium six set. assessments included electrochemical impedance spectroscopy (EIS) potentiodynamic scanning (PDS) techniques. results indicate that borate buffer improves protection primers more effectively than phosphate mixed ones.

Language: Английский

Citations

1