Electromigration Techniques in the Analysis of Selected Cosmetic Ingredients: A Review

Molecules, Journal Year: 2025, Volume and Issue: 30(1), P. 161 - 161

Published: Jan. 3, 2025

The cosmetics industry is one of the fastest-growing sectors worldwide. dynamic evolution this results in an increasingly diverse range products containing various active ingredients. Ensuring quality these crucial for consumer safety, necessitating use advanced analytical methods and adherence to legal regulations. Electrophoretic techniques, particularly capillary electrophoresis micellar electrokinetic chromatography, facilitate rapid precise separation identification cosmetic A well-chosen technique optimized conditions ensure high sensitivity, repeatability, resolution, achieving detection limits that meet requirements. Although electromigration techniques are less common routine laboratory analyses compared liquid they show potential broader application analyzing substances found cosmetics. This study reviews possibilities applying different electrophoretic analyze selected ingredients serving functions, including preservatives, dyes, exfoliating agents, UV filters, also contaminants, while considering sample preparation methods, equipment used, analysis conditions. compiled data indicate electrophoresis, when high-performance chromatography ion shows comparable or superior sensitivity with adequate regulatory standards.

Language: Английский

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Novel developments in capillary electrophoresis miniaturization, sampling, detection and portability: An overview of the last decade

TrAC Trends in Analytical Chemistry, Journal Year: 2023, Volume and Issue: 159, P. 116941 - 116941

Published: Jan. 17, 2023

Language: Английский

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Recent progress in photoelectrochemical sensors to quantify pesticides in foods: Theory, photoactive substrate selection, recognition elements and applications

TrAC Trends in Analytical Chemistry, Journal Year: 2023, Volume and Issue: 164, P. 117108 - 117108

Published: May 20, 2023

Language: Английский

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Progress in on-line, at-line, and in-line coupling of sample treatment with capillary and microchip electrophoresis over the past 10 years: A review

Analytica Chimica Acta, Journal Year: 2023, Volume and Issue: 1261, P. 341249 - 341249

Published: April 22, 2023

Language: Английский

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Current green capillary electrophoresis and liquid chromatography methods for analysis of pharmaceutical and biomedical samples (2019–2023) – A review

Analytica Chimica Acta, Journal Year: 2024, Volume and Issue: 1323, P. 342889 - 342889

Published: June 20, 2024

Separation analytical methods, including liquid chromatography (LC) and capillary electrophoresis (CE), in combination with an appropriate detection technique, are dominant powerful approaches preferred the analysis of pharmaceutical biomedical samples. Recent trends methods focused on activities that push them to field greenness sustainability. New based implementation greener solvents, non-hazardous chemicals, reagents have grown exponentially. Similarly, recent pushed strategies miniaturization, reduction wastes, avoiding derivatization procedures, or energy consumption. However, real method can be evaluated only according objective sufficient metric offering complex results taking into account all twelve rules green chemistry (SIGNIFICANCE mnemonic system). This review provides extensive overview papers published area development LC CE over last 5 years (2019-2023). The main focus is situated metrics used for evaluation applied determination bioactive agents. It critically evaluates compares demands applicability quality control clinical environment requirements (GAC). Greenness practicality summarized re-evaluated newly use tools, i.e., Analytical GREEnness (AGREE), Green Procedure Index (GAPI), Blue Applicability Grade (BAGI), Sample Preparation Metric Sustainability (SPMS). Moreover, general conclusions future perspectives greening procedures systems presented. paper should provide comprehensive information chemists, biochemists, it also represent a valuable source clinicians, laboratories interested greenness, practicality,

Language: Английский

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Recent developments and applications of capillary and microchip electrophoresis in proteomics and peptidomics (mid‐2018–2022)

Journal of Separation Science, Journal Year: 2023, Volume and Issue: 46(12)

Published: Feb. 26, 2023

This review gives a wide overview of recent advances and applications capillary electrophoresis microchip methods in the fields proteomics peptidomics period from mid‐2018 up to end 2022. The methodological topics covering sample preparation concentration techniques, hyphenation with mass spectrometry, multidimensional separations by on‐line or off‐line coupled different liquid chromatography techniques are described new developments both bottom‐up top‐down approaches presented. In addition, various proteomic peptidomic studies demonstrated. They include monitoring protein posttranslational modifications biological biochemical research, clinical proteomics, food analysis.

Language: Английский

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Microfluidics for COVID-19: From Current Work to Future Perspective

Biosensors, Journal Year: 2023, Volume and Issue: 13(2), P. 163 - 163

Published: Jan. 20, 2023

Spread of coronavirus disease 2019 (COVID-19) has significantly impacted the public health and economic sectors. It is urgently necessary to develop rapid, convenient, cost-effective point-of-care testing (POCT) technologies for early diagnosis control plague’s transmission. Developing POCT methods related devices critical achieving diagnosis. With advantages miniaturization, high throughput, small sample requirements, low actual consumption, microfluidics an essential technology development devices. In this review, according different driving forces fluid, we introduce common based on microfluidic market, including paper-based microfluidic, centrifugal optical digital platforms. Furthermore, various microfluidic-based assays diagnosing COVID-19 are summarized, immunoassays, such as ELISA, molecular assays, PCR. Finally, challenges future perspectives device design presented. The ultimate goals paper provide new insights directions diagnostics while expecting contribute COVID-19.

Language: Английский

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Genetic diversity and population structure of Polygonatum cyrtonema Hua in China using SSR markers

PLoS ONE, Journal Year: 2023, Volume and Issue: 18(8), P. e0290605 - e0290605

Published: Aug. 31, 2023

Polygonatum cyrtonema Hua is a perennial herbaceous plant of the genus, belonging to Liliaceae family, with significant medicinal and nutritional value. In China, this species traditional edible herb long history application widely appreciated by people. However, as demand for herbs continues grow, excessive harvesting has led depletion wild resources risk genetic erosion. addition, chaotic cultivation varieties lack high quality germplasm have inconsistent medical materials. Therefore, it urgent conduct diversity evaluation establish sound conservation plan. This study assessed population structure 96 samples collected from seven regions in China using simple sequence repeat (SSR) molecular marker technology. study, total 60 alleles (Na) were detected across 10 polymorphic SSR markers used, an average 6.0 generated per locus. The values information content (PIC) ranged 0.3396 0.8794, value 0.6430. effective number (Ne) was 2.761, Shannon's index (I) 1.196. analysis indicates that can be classified into three subpopulations (JZ, QY, JD) at level, which corresponds previous subgroups identified based on individual phenotypic traits. Analysis Molecular Variance (AMOVA) showed 74% variation between individuals within populations different regions. phylogenetic divided them main populations. QY JD are largely clustered together, could attributed their mountainous distribution local climate environment. differentiation coefficient (Fst) low 0.065, indicating relatively differentiation. ratio JZ other two (QY much higher than Based clustering results (Fst), inferred relationship closer, certain degree subpopulation. supports provides new parental material improvement breeding programs.

Language: Английский

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Capillary electrophoresis tandem mass spectrometry to determine multiclass cyanotoxins in reservoir water and spinach samples

Journal of Chromatography A, Journal Year: 2024, Volume and Issue: 1717, P. 464666 - 464666

Published: Jan. 22, 2024

Cyanotoxins constitute a group of toxic secondary metabolites, the presence which in any water body poses major health risk. Moreover, advanced organisms such as edible plants exposed to these toxins, are possible pathway for human exposure. Green analytical chemistry is demanding environmentally friendly techniques. In this sense, we propose use capillary electrophoresis coupled tandem mass spectrometry (CE-MS/MS) determine mixture eight cyanotoxins belonging three different classes: cyclic peptides (microcystin-LR, microcystin-RR and nodularin), alkaloids (cylindrospermopsin anatoxin-a) isomeric non-protein amino acids (β-methylamino-L-alanine, 2,4-diaminobutyric acid N-(2-aminoethyl)glycine). Separation was achieved by using an acidic background electrolyte consisting 2 M formic 20 % acetonitrile water. Parameters affecting MS/MS detection sheath-liquid interface were also studied. Finally, combination pH-junction, field-amplified sample stacking (FASS) barrage online preconcentration strategies, employed improve sensitivity efficiency. The applied, with dual cartridge solid-phase extraction (SPE) system, allows obtain limits very low range µg·L−1 multiclass reservoir samples (from 0.005 0.10 µg·L−1). Furthermore, first time analysed spinach through CE-MS/MS same SPE procedure, following lyophilisation solid-liquid 6 mL 80% aqueous MeOH.

Language: Английский

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Factors influencing the quality of Royal jelly and its components: a review

Cogent Food & Agriculture, Journal Year: 2024, Volume and Issue: 10(1)

Published: May 9, 2024

Royal jelly (RJ) has various applications in cosmetics, health food, and apitherapy to treat chronic inflammation disorders. It is a milky white substance rich proteins, carbohydrates, lipids, vitamins, minerals. RJ acts as an antioxidant, anti–inflammatory, antimicrobial agent, which helps reducing boosting immunity. This review provides insight into the sensory chemical analytical aspects of RJ, with focus on water, 10–hydroxy–2–decenoic acid (10–HDA), protein, sugar contents, well national international quality standards major honey–producing countries. The composition varies across locations due external conditions, nectar sources, harvesting honeybee species, affect its quantity quality. Despite having consistent composition, production per colony influenced by environmental source attributes, mineral, vitamin, amino content. Advanced methods are required accurately quantify diverse ingredients responsible for biological pharmacological effects. Understanding intricacies essential unlock therapeutic potential. Notably, apiculture research at level sensitive bioindicators, emphasizing global need standards. exploration contributes understanding how factors bee product

Language: Английский

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