Microwave-Assisted Silanization of Magnetite Nanoparticles Pre-Synthesized by a 3D Microfluidic Platform DOI Creative Commons
Adelina-Gabriela Niculescu, Alina Moroșan, Alexandra Cătălina Bîrcă

et al.

Nanomaterials, Journal Year: 2023, Volume and Issue: 13(20), P. 2795 - 2795

Published: Oct. 20, 2023

Magnetite nanoparticles (Fe3O4 NPs) are among the most investigated nanomaterials, being recognized for their biocompatibility, versatility, and strong magnetic properties. Given that applicability depends on dimensions, crystal morphology, surface chemistry, Fe3O4 NPs must be synthesized in a controlled, simple, reproducible manner. Since conventional methods often lack tight control over reaction parameters produce materials with unreliable characteristics, increased scientific interest has been directed to microfluidic techniques. In this context, present paper describes development of an innovative 3D platform suitable synthesizing uniform fine-tuned On-chip co-precipitation was performed, followed by microwave-assisted silanization. The obtained were characterized from compositional microstructural perspectives X-ray diffraction (XRD) transmission electron microscopy (TEM). Moreover, supplementary physicochemical investigations, such as Fourier Transform Infrared Spectroscopy (FT-IR), Kaiser Test, Ultraviolet-Visible (UV-Vis) Spectrophotometry, Dynamic Light Scattering (DLS), Thermogravimetry Differential Scanning Calorimetry (TG-DSC) analyses, demonstrated successful modification. Considering positive results, presented synthesis functionalization method represents fast, reliable, effective alternative producing tailored nanoparticles.

Language: Английский

Formulation and Characterization of Fe3O4@PEG Nanoparticles Loaded Sorafenib; Molecular Studies and Evaluation of Cytotoxicity in Liver Cancer Cell Lines DOI Open Access
Mona Ebadi, Ahmad Rifqi Md Zain, Tengku Hasnan Tengku Abdul Aziz

et al.

Polymers, Journal Year: 2023, Volume and Issue: 15(4), P. 971 - 971

Published: Feb. 16, 2023

Iron oxide nanoparticles are one of the nanocarriers that suitable for novel drug delivery systems due to low toxicity, biocompatibility, loading capacity, and controlled cancer cells. The purpose present study is synthesis coated iron sorafenib (SFB) its effects on In this study, Fe3O4 were synthesized by co-precipitation method, then was loaded onto PEG@Fe3O4 nanoparticles. FTIR used ensure polyethylene glycol (PEG) binding nanoshells. A comparison mean size crystalline structure performed TEM, DLS, X-ray diffraction patterns. Then, cell viability obtained MTT assay 3T3 HepG2 lines. According FT-IR results, presence O-H C-H bands at 3427 cm-1 1420 peak correlate with PEG XRD pattern showed cubic spinel trapped magnetite carrying medium. magnetic properties examined a vibrating-sample magnetometer (VSM). IC50 values 72 h treatment carriers Fe3O4@PEG nanoparticle line 15.78 μg/mL (p < 0.05). This using them in process could be beneficial increasing effect

Language: Английский

Citations

18
Bimagnetic hard/soft and soft/hard ferrite nanocomposites: Structural, magnetic and hyperthermia properties DOI

H. Jalili,

B. Aslibeiki, Abdollah Hajalilou

et al.

Ceramics International, Journal Year: 2021, Volume and Issue: 48(4), P. 4886 - 4896

Published: Nov. 5, 2021

Language: Английский

Citations

39
3D printed superparamagnetic stimuli-responsive starfish-shaped hydrogels DOI Creative Commons
Ali A. Mohammed,

Jingqi Miao,

Ieva Ragaisyte

et al.

Heliyon, Journal Year: 2023, Volume and Issue: 9(4), P. e14682 - e14682

Published: March 28, 2023

Magnetic-stimuli responsive hydrogels are quickly becoming a promising class of materials across numerous fields, including biomedical devices, soft robotic actuators, and wearable electronics. Hydrogels commonly fabricated by conventional methods that limit the potential for complex architectures normally required rapidly changing custom configurations. Rapid prototyping using 3D printing provides solution this. Previous work has shown successful extrusion magnetic hydrogels; however, extrusion-based is limited nozzle resolution ink viscosity. VAT photopolymerization offers higher control over build-architecture. Liquid photo-resins with nanocomposites suffer from nanoparticle agglomeration due to local fields. In this work, we develop an optimised method homogenously infusing up 2 wt % superparamagnetic iron oxide nanoparticles (SPIONs) 10 nm diameter into photo-resin composed water, acrylamide PEGDA, improved homogeneity reduced during printing. The printed starfish exhibited high mechanical stability robust properties maximum Youngs modulus 1.8 MPa shape deformation 10% when swollen. Each individual arm could be magnetically actuated remote field applied. grab onto magnet all arms central was Ultimately, these retained their post-printing returned original formation once had been removed. These can used wide range applications, robotics stimulated actuators.

Language: Английский

Citations

15
Comprehensive in-vitro and magnetic hyperthermia investigation of biocompatible non-stoichiometric Zn0.5Ca0.5Fe2O4 and Mg0.5Ca0.5Fe2O4 nanoferrites on lung cancer cell lines DOI

Sudeep Tiwari,

Pragya Joshi,

Krishna Priya Hazarika

et al.

Journal of Alloys and Compounds, Journal Year: 2023, Volume and Issue: 972, P. 172588 - 172588

Published: Oct. 20, 2023

Language: Английский

Citations

15
Preparation, physicochemical characterization, and AC induction heating properties of colloidal aggregates of ferrimagnetic cobalt ferrite nanoparticles coated with a bio-compatible polymer DOI

I. Anila,

B.B. Lahiri,

Subin P. John

et al.

Ceramics International, Journal Year: 2023, Volume and Issue: 49(10), P. 15183 - 15199

Published: Jan. 13, 2023

Language: Английский

Citations

13
Optical, microstructural, and magnetic hyperthermia properties of green-synthesized Fe3O4/carbon dots nanocomposites utilizing Moringa oleifera extract and watermelon rinds DOI Creative Commons

Adhistinka Jiananda,

Emi Kurnia Sari,

Dyah Ayu Larasati

et al.

Carbon Trends, Journal Year: 2023, Volume and Issue: 13, P. 100305 - 100305

Published: Oct. 15, 2023

Cancer therapy with targeted-localized heating is one of the breakthroughs in biomedical field. The incorporation magnetic nanoparticles and fluorescent was crucial issues for hyperthermia applications. This research investigates properties green-synthesized Fe3O4/CDs. Fe3O4 were synthesized using coprecipitation method Moringa oleifera leaf extract as a reducing agent stabilizer. In contrast, CDs hydrothermal watermelon rind waste carbon source. X-ray diffraction analysis confirmed presence cubic inverse spinel reduction crystallite size increasing concentration. Transmission electron microscopy revealed particle distributions 9.7 nm 7.5 Scanning showed that distributed on surface Fe3O4. detection characteristic Fe-O, C=C, C-O, C-O-C bonds indicated Ultraviolet-visible spectroscopy spectra absorption peaks at 282 193 Photoluminescence shifts from 509 to 505 excitation wavelength both Fe3O4/CDs, situated within green region visible light. vibrating sample magnetometer nanocomposites displayed characteristics soft ferromagnetic materials. Furthermore, specific rate (SAR) value Fe3O4/CDs found be dependent magnetization. SAR decreased concentration increased, frequency strength AMF increased. Therefore, these results can promote promising candidate

Language: Английский

Citations

11
Effect of ligand dispersant on superparamagnetic heating capacity and cytotoxicity properties of MnFe2O4 nanoparticles DOI
V. Vijayakanth, C. Krishnamoorthi

Journal of Materials Science Materials in Electronics, Journal Year: 2024, Volume and Issue: 35(6)

Published: Feb. 1, 2024

Language: Английский

Citations

4
Iron-Based Ceramic Composite Nanomaterials for Magnetic Fluid Hyperthermia and Drug Delivery DOI Creative Commons
Ming‐Hsien Chan, Chien‐Hsiu Li, Yu‐Chan Chang

et al.

Pharmaceutics, Journal Year: 2022, Volume and Issue: 14(12), P. 2584 - 2584

Published: Nov. 24, 2022

Because of the unique physicochemical properties magnetic iron-based nanoparticles, such as superparamagnetism, high saturation magnetization, and effective surface area, they have been applied in biomedical fields diagnostic imaging, disease treatment, biochemical separation. Iron-based nanoparticles used resonance imaging (MRI) to produce clearer more detailed images, therapeutic applications fluid hyperthermia (MFH). In recent years, researchers clay minerals, ceramic materials with construct nanocomposite enhanced saturation, thermal effects. Owing their structure large specific can be homogenized by adding different proportions minerals before after modification enhance magnetization. this review, we assess potential improve preparation multifunctional composite through combination materials. We demonstrate ferromagnetic enhancement for MRI diagnosis, drug delivery, MFH therapy, cellular applications.

Language: Английский

Citations

15
Electron spin resonance and induction heating studies of zinc substituted (Mn, Co) ferrite nanoparticles for potential magnetic hyperthermia applications DOI
L.C. Sonia, Goutam Singh Ningombam, Sumitra Phanjoubam

et al.

Journal of Alloys and Compounds, Journal Year: 2023, Volume and Issue: 946, P. 169327 - 169327

Published: Feb. 16, 2023

Language: Английский

Citations

9
Novel green synthesis approach of Fe3O4-MSN/Ag nanocomposite using moringa oleifera extract for magnetic hyperthermia applications DOI
Mahardika Yoga Darmawan,

Marhan Ebit Saputra,

Leni Rumiyanti

et al.

Current Applied Physics, Journal Year: 2024, Volume and Issue: unknown

Published: Oct. 1, 2024

Language: Английский

Citations

2