In
this
study,
nano
Ti/AZ31
magnesium
matrix
composites
were
successfully
prepared
by
powder
metallurgy
method,
and
the
strength
plasticity
of
improved
in
both
directions.
The
SEM
test
shows
that
Ti
particles
evenly
distributed
at
grain
boundary
sintered
composite,
pin
to
make
composite
significantly
refined.
EBSD
addition
reduces
texture
increases
starting
probability
slip
system.
TEM
showed
AZ31
formed
stable
Al3Ti
MgO
phases
interface,
a
strong
coherent
relationship.
nanoindentation
interface
was
stable,
bonding
energy
fracture
toughness
gradiently
distributed,
area
better
than
those
matrix.
Tensile
tests
state
1.5wt.%Ti/AZ31
presented
best
mechanical
properties
with
yield
strength,
ultimate
tensile
elongation
143
MPa,
243
MPa
11.5%,
obviously
higher
alloys.
increased
mainly
due
refinement
strengthening
boundaries.
ductility
result
weakened
texture,
increase
system
start-up
interfacial
between
Journal of Materials Research and Technology,
Journal Year:
2023,
Volume and Issue:
26, P. 8569 - 8603
Published: Sept. 1, 2023
Aluminium
(Al)
Alloy-6061/TiB2
was
developed
with
Squeeze
casting
while
varying
composite
quantities
titanium
diboride
(TiB2).
The
metallographic
structure
of
the
investigated
using
EDS
and
scanning
electron
microscopy
(SEM).
machining
is
challenging
conventional
methods
due
to
higher
tool
wear
surface
roughness
(Ra).
This
study
analyses
output
responses,
machinability
TiB2
15%
volume
reinforced
AA6061
composites
Electrical
Discharge
Machining
(EDM).
EDM
operation
variables
such
as
current,
pulse
on
time,
voltage
gap
were
utilized
examine
material
removal
rate
(MRR),
(TWR)
Ra
employing
Box–Behnken
design
experiments.
MRR,
TWR
data
acquired
from
various
experiments
optimized
considering
single
multiple
objectives
by
a
hybrid
approach.
Machine
learning
(ML)
applied
predict
responses
linear
regression
(LR),
decision
tree
(DT)
random
forest
(RF).
samples'
recast
layer
examined
SEM,
thickness
also
documented.
Al6061
alloy's
SEM
micrographs
reveal
deep
equiaxed
dimples
its
fracture
surface,
indicating
high
level
plastic
deformation
before
failure.
evenly
distributed
darker
particles
in
Al-matrix
alloy
no
directional-orientation.
Al6061-15
wt%
composites'
surfaces
display
dimples,
ductile-fracture
for
deformation,
cleavage
facets
some
areas.
aluminum
pattern
depicts
long,
extensive
ploughing
grooves
short
cracks
parallel
sliding
direction
at
grooves'
bottom.
recast-layer
formation
have
reported
that
molten
metal
ligaments
break
into
droplets
during
flushing,
exposing
fresh
surfaces.
groove
width
larger
compared
composites.
Thus,
it
can
be
observed
tracks
base
are
deeper
comparison
Al-
15
presence
hard
particles.
Also,
may
advantageous
wear-resistant
properties.
has
importance
an
industry
where
components
slide
each
other
used
disc
brakes
automobiles.
Compared
standards,
single-objective
optimization
considerably
enhanced
outcomes:
MRR
increased
10.61%,
enriched
25.91%,
17.60%.
According
ANOVA,
peak
current
contributed
87.88%,
98.18%,
95.80%
respectively
TWR,
Ra.
It
requisite
investigate
multi-objective
owing
diverse
optimal
factor
combinations
responses.
slightly
1.14%
simultaneous
utilizing
techniques
Equal
Entropy
weights,
which
diminished
11.74%
11.66%.
ML,
particularly
DT,
improves
performance
assisting
productivity,
durability,
cost-efficiency
under
changeable
circumstances
raising
forthcoming
possibilities.
Journal of Materials Research and Technology,
Journal Year:
2023,
Volume and Issue:
28, P. 4299 - 4316
Published: Dec. 30, 2023
The
microstructure,
homogeneity,
and
tribo-corrosion
behavior
of
microwave-developed
Nickel
as
well
titanium
dioxide
SS-304
cladding
surfaces
are
the
primary
emphasis
this
research.
study
includes
assessing
hardness
enhancement
from
Ni
TiO2
particles
in
surface.
investigation
additionally
evaluates
surface
wear
rates,
friction
coefficients,
resistance
to
corrosion
under
tribological
conditions.
with
developed
by
microwave
energy
were
investigated
study.
microstructure
was
being
examined
validate
uniformly
homogeneous
dispersion
particles,
XRD
employed
determine
phases.
evaluated,
a
pin-on-disk
tribometer
has
assessed
behavior.
Tribo-corrosion
tested
3.5-percent
NaCl
solution.
To
enhance
cladding's
efficiency,
hybrid
heating
(MHH)
utilising
charcoal
susceptor
been
employed.
Findings
exhibited
that
analysis
showed
had
uniform
distribution
compact
microstructure.
significantly
improved
about
37.68%
due
incorporation
10%
particles.
FeNi3,
NiSi2,
Ni3C,
NiC,
Ni2Si,
FeNi,
phases
seen
on
conditions
also
evaluated
using
tribometer.
outcomes
have
decreased
rates
coefficients
compared
uncoated
substrate.
Moreover,
3.5%
rate
coefficient
measured
be
0.00412
mm3/m
0.297,
respectively.
results
indicated
enhanced
Journal of Manufacturing and Materials Processing,
Journal Year:
2024,
Volume and Issue:
8(2), P. 58 - 58
Published: March 8, 2024
The
utilization
of
Al2O3
nanopowder
to
reinforce
AA5754
aluminum
alloy
through
blind
holes
employing
the
friction
stir
processing
(FSP)
technique
produce
an
matrix
nanocomposite
is
explored
in
this
paper.
Motivated
by
necessity
enhance
strength
and
ductility
welded
joints,
impacts
varying
tool
rotational
speed
(rpm)
hole
diameter
on
microstructure
mechanical
properties
joints
are
investigated.
Experimental
characterization
techniques
including
SEM,
optical
microscopy,
microhardness,
tensile
tests
were
employed
analyze
produced
under
different
parameters
(tool
speeds
910,
1280,
1700
rpm,
diameters
0,
1,
1.5,
2
mm).
Comparative
analyses
conducted
against
base
metal
without
reinforcement
powder.
It
was
found
that
addition
resulted
a
decrease
maximum
generated
heat
during
FSP,
while
also
reducing
zone
size
compared
samples
nanopowder.
Moreover,
enhancements
both
observed
with
incorporation
nanoparticles.
optimal
combination
welding
conditions,
at
1280
rpm
1.5
mm
diameter,
yielded
remarkable
ultimate
567
MPa,
accompanied
hardness
45
HV.
These
results
underscore
potential
nano-Al2O3
significantly
improving
nanocomposite,
implications
for
advancing
performance
structures
various
engineering
applications.
Journal of Magnesium and Alloys,
Journal Year:
2024,
Volume and Issue:
12(6), P. 2091 - 2146
Published: June 1, 2024
Rising
concerns
about
climate
change
drive
the
demand
for
lightweight
components.
Magnesium
(Mg)
alloys
are
highly
valued
their
low
weight,
making
them
increasingly
important
in
various
industries.
Researchers
focusing
on
enhancing
characteristics
of
Mg
and
developing
Metal
Matrix
Composites
(MMCs)
have
gained
significant
attention
worldwide
over
past
decade,
driven
by
global
shift
towards
materials.
Friction
Stir
Processing
(FSP)
has
emerged
as
a
promising
technique
to
enhance
properties
produce
Mg-MMCs.
Initially,
FSP
adapted
refine
grain
size
from
micro
nano
level
accelerated
development
MMCs
due
its
solid-state
nature
synergistic
effects
microstructure
refinement
reinforcement,
improving
strength,
hardness,
ductility,
wear
resistance,
corrosion
fatigue
strength.
However,
producing
defect-free
sound
FSPed
Mg-MMCs
requires
addressing
several
variables
interdependencies,
which
opens
up
broad
range
practical
applications.
Despite
existing
reviews
individual
Mg,
alloys,
MMCs,
an
attempt
been
made
analyze
latest
research
these
three
aspects
collectively
understanding,
application,
effectiveness
derivatives.
This
review
article
discusses
literature,
classifies
importance
provides
historical
background,
explores
developments
potential
applications
alloys.
It
focuses
novel
fabrication
methods,
reinforcement
strategies,
machine
tool
design
parameters,
material
characterization,
integration
with
other
methods
enhanced
properties.
The
influence
process
parameters
emergence
defects
examined,
along
specific
mono
hybrid
composites
evolution.
study
identifies
materials
highlights
gaps
production.
concludes
recommendations
further
exploration,
reflecting
ongoing
advancements
this
field.
Journal of Materials Research and Technology,
Journal Year:
2023,
Volume and Issue:
24, P. 9984 - 10004
Published: May 1, 2023
The
mixture
of
the
rare-earth
CeO2
and
ZrO2
particulates
was
used
for
fabricating
hybridized
AZ31BMg/(CeO2+ZrO2)p
composites
by
utilizing
friction
stir
processing
with
a
multiple-tool
pass
strategy.
structure,
mechanical
properties
(tensile
strength
hardness),
tribological
performances
(wear
properties)
corrosion
behaviours
hybrid
were
examined.
findings
reveal
elimination
tunnel-like
defects
clustering
CeO2+ZrO2
particles
in
composite
after
multiple
passes
tool
due
to
successive
stirring-assisted
material
flow.
rise
reduced
mean
grain
sizes
(7.91–3.02
μm),
particle
(5.47–2.28
average
coefficient
(0.45–0.18)
specific
wear
rate
(4.26
×
10−5–2.17
10−5
mm3/Nm)
composite.
tensile
(172–239
MPa),
performance
also
improved
via
Multiple
is
thus
recommended
fabrication
Mg-based
composites.
Journal of Materials Research and Technology,
Journal Year:
2023,
Volume and Issue:
28, P. 1891 - 1899
Published: Dec. 9, 2023
In
this
work,
the
AZ31
Mg
alloy
was
subjected
to
friction
stir
processing
(FSP)
by
adding
CuO
and
ZrO2
particles.
The
main
aim
of
study
increase
tribological
mechanical
behavior
AZ
31/(CuO
+
ZrO2)p
surface
composite
in
air
water.
influence
media
on
microstructural
modification
properties
developed
composites
is
assessed
via
optical
microscopy
(OM),
scanning
electron
(SEM),
transmission
(TEM),
shear
punch
testing
(SPT)
Vickers
hardness
testing.
It
had
been
found
that
finer
grains
are
produced
zone
due
reduction
heat
input
for
water-cooled
relative
air-cooled
composite.
Indeed,
water-cooling
system
acted
as
a
hamper
suppressed
grain
growth,
which
consequently
resulted
enhancement
Journal of Materials Research and Technology,
Journal Year:
2023,
Volume and Issue:
27, P. 852 - 875
Published: Sept. 27, 2023
In
the
present
study,
an
Mg-based
biomedical
composite
is
fabricated
by
addition
of
Hydroxyapatite
bioactive
nanoparticles
into
a
substrate
bioabsorbable
WE43
Mg
alloy
using
multi
pass
friction
stir
processing
(FSP).
The
findings
indicate
that
applying
6
passes
FSP
leads
to
decrease
grain
size
over
93%,
crushing
and
redistribution
secondary
phase
particles
within
matrix,
improved
homogeneity
reduction
in
their
agglomeration.
vitro
Biodegradation
tests
prove
as
number
increases,
weight
loss
bio-composites
biodegradation
rate
simulated
body
fluid
(SBF)
decrease.
Bioactivity
assessed
immersion
SBF
for
28
days.
Biomineralization
process
shows
all
Mg-Hydroxyapatite
exhibit
bone-like
apatite
forming
ability,
cauliflower-shaped
crystals
form
on
surface.
Moreover,
increasing
uniformity
stimulates
formation
denser
crystals,
which
improves
biocompatibility
bio-composites.
Biocompatibility
also
evaluated
MTT
assay
DAPI
staining.
Mg-HA-6P
demonstrates
highest
healthy
flattened
spindle
shaped
L-929
fibroblast
cells
with
83.36%
cell
viability
after
5
days
incubation
compared
other
samples.
Increasing
causes
high
bioactivity,
low
homogenous
distribution
particles,
turn
improve
cells.
Furthermore,
increase
passes,
yield
strength
values
samples
increase,
reaching
212
MPa
226
Mg-6P
Mg-6P-HA
samples,
respectively.
Composite Interfaces,
Journal Year:
2023,
Volume and Issue:
31(3), P. 305 - 330
Published: Sept. 18, 2023
ABSTRACTIn
the
present
study,
Behavior
of
Dissimilar
A356-AZ91/CeO2
Aluminum-Magnesium
Based
Composite
Fabricated
by
Friction
Stir
Process
Technique
was
observed.
The
Macrostructure
A356-AZ91/5%CeO2/2%
Ni
showed
a
defect-free
and
crack-free
composite.
Microstructural
examination
revealed
that
FSP
effectively
distributed
CeO2
particles
within
matrix,
resulting
in
refined
microstructure.
Tensile
strength
A356-AZ91
matrix
material
improved
about
38.04%
after
addition
5%
CeO2.
However,
with
2%
to
A356-AZ91/5%
composite
displaying
further
enhancement.
alloy
through
44.78%
improvement
tensile
strength.
There
an
hardness
adding
Ni-
found
41.66%.
Hardness
A356-AZ91-5%
only
28.33%
without
Ni.
Wear
testing
aluminum
carried
out
using
pin-on-disc
apparatus.
wear
rate
decreased
70%
particles.
61.66%
particles.KEYWORDS:
Interfacial
layermacrostructureFSP
techniquefatigue
strengthwear
Disclosure
statementNo
potential
conflict
interest
reported
author(s).