Evaluating the Role of Metastable Surfaces in Mechanochemical Reduction of Molybdenum Oxide DOI Creative Commons

Neung-Kyung Yu,

Letícia F. Rasteiro, Van Son Nguyen

et al.

JACS Au, Journal Year: 2024, Volume and Issue: unknown

Published: Nov. 19, 2024

Mechanochemistry and mechanocatalysis are gaining increasing attention as environmentally friendly chemical processes because of their solvent-free nature scalability. Significant effort has been devoted for studying continuum-scale phenomena in mechanochemistry, such temperature pressure gradients, but the atomic-scale mechanisms remain relatively unexplored. In this work, we focus on mechanochemical reduction MoO3 a case study. We use experimental techniques to determine conditions density functional theory (DFT) simulations establish an atomistic framework identifying metastable surfaces that most likely enable process. Our results show can significantly lower or remove thermodynamic barriers surface kinetic energy from milling facilitate formation have high fracture energies not thermally accessible. These findings indicate important aspect mechanochemistry along with hot spots other phenomena.

Language: Английский

Understanding Free-Energy Landscapes in Electrocatalysis: A Case Study on Nitrate Reduction over Au(111) DOI Creative Commons
Ebrahim Tayyebi, Kai S. Exner

ACS electrochemistry., Journal Year: 2025, Volume and Issue: unknown

Published: Feb. 25, 2025

Free-energy landscapes are essential tools in electrocatalysis for assessing catalyst activity and selectivity of proton-coupled electron transfer steps. It is a common approach to focus on the thermodynamic part free-energy landscape refer only reaction intermediates, which turn leads results being highly dependent accuracy calculated binding energies adsorbed intermediates. Since evaluation electrocatalytic processes solid surfaces usually requires density functional theory calculations (DFT) with periodic boundary conditions, free energy reference molecules relevant binding-energy determination subject an inherent error. For this purpose, gas-phase error corrections have been introduced recent years, allow correction DFT error, based assessment formation enthalpies, by assigning double or triple bonds molecules. In contribution, we present simple unbiased errors: do not distinguish between bond order but correct all single, double, referring atomization compounds. We employ our nitrate reduction Au(111) as case study, using different levels exchange–correlation functionals generalized gradient meta-generalized approximation. shown that inclusion well solvation ion significantly affects energetics predictions descriptor-based analysis, highlighting importance correcting DFT-based gaining reliable insights into systems.

Language: Английский

Citations

1

Sustainable carbon electrode materials from biomass for redox flow batteries DOI
Tholkappiyan Ramachandran, Rajwali Khan, Avijit Ghosh

et al.

Biomass and Bioenergy, Journal Year: 2025, Volume and Issue: 198, P. 107846 - 107846

Published: April 9, 2025

Language: Английский

Citations

0

Unifying thermochemistry concepts in computational heterogeneous catalysis DOI Creative Commons
Bjarne Kreitz, Gabriel S. Gusmão, Dingqi Nai

et al.

Chemical Society Reviews, Journal Year: 2024, Volume and Issue: unknown

Published: Nov. 29, 2024

Thermophysical properties of adsorbates and gas-phase species define the free energy landscape heterogeneously catalyzed processes are pivotal for an atomistic understanding catalyst performance.

Language: Английский

Citations

2

Unifying thermochemistry concepts in computational heterogeneous catalysis DOI Creative Commons
Bjarne Kreitz, Gabriel S. Gusmão, Dingqi Nai

et al.

Published: Aug. 2, 2024

Thermophysical properties of adsorbates and gas-phase species define the free energy landscape heterogeneously catalyzed processes are pivotal for an atomistic understanding catalyst performance. These thermophysical properties, such as or enthalpy, typically derived from density functional theory (DFT) calculations. Enthalpies species-interdependent that only meaningful when referenced to other species. The widespread use DFT has led a proliferation new energetic data in literature databases. However, there is lack consistency how associated enthalpies energies stored reported, leading challenges reproducing utilizing results prior work. Additionally, suffers exchange-correlation errors often require corrections align with global thermochemical networks, which not always clearly documented explained. In this review, we introduce set consistent terminology definitions, review existing approaches, unify techniques using framework linear algebra. This tools facilitates correction alignment between different formats sources, promoting sharing reuse ab initio data. Standardization thermochemistry concepts computational heterogeneous catalysis reduces cost enhances fundamental catalytic processes, will accelerate design optimally performing catalysts.

Language: Английский

Citations

1

Uncertainty quantification and propagation in atomistic machine learning DOI Creative Commons
Jin Dai, Santosh Adhikari, Mingjian Wen

et al.

Reviews in Chemical Engineering, Journal Year: 2024, Volume and Issue: unknown

Published: Dec. 30, 2024

Abstract Machine learning (ML) offers promising new approaches to tackle complex problems and has been increasingly adopted in chemical materials sciences. In general, ML models employ generic mathematical functions attempt learn essential physics chemistry from large amounts of data. The reliability predictions, however, is often not guaranteed, particularly for out-of-distribution data, due the limited physical or principles functional form. Therefore, it critical quantify uncertainty predictions understand its propagation downstream applications. This review examines existing quantification (UQ) (UP) methods atomistic under framework probabilistic modeling. We first categorize UQ explain similarities differences among them. Following this, performance metrics evaluating their accuracy, precision, calibration, efficiency are presented, along with techniques recalibration. These then applied survey benchmark studies that use molecular datasets. Furthermore, we discuss UP propagate widely used simulation techniques, such as dynamics microkinetic conclude remarks on challenges opportunities ML.

Language: Английский

Citations

1

Evaluating the Role of Metastable Surfaces in Mechanochemical Reduction of Molybdenum Oxide DOI Creative Commons

Neung-Kyung Yu,

Letícia F. Rasteiro, Van Son Nguyen

et al.

JACS Au, Journal Year: 2024, Volume and Issue: unknown

Published: Nov. 19, 2024

Mechanochemistry and mechanocatalysis are gaining increasing attention as environmentally friendly chemical processes because of their solvent-free nature scalability. Significant effort has been devoted for studying continuum-scale phenomena in mechanochemistry, such temperature pressure gradients, but the atomic-scale mechanisms remain relatively unexplored. In this work, we focus on mechanochemical reduction MoO3 a case study. We use experimental techniques to determine conditions density functional theory (DFT) simulations establish an atomistic framework identifying metastable surfaces that most likely enable process. Our results show can significantly lower or remove thermodynamic barriers surface kinetic energy from milling facilitate formation have high fracture energies not thermally accessible. These findings indicate important aspect mechanochemistry along with hot spots other phenomena.

Language: Английский

Citations

0