Application of Sulfonyl Fluorides in Organic Transformation DOI
Sichang Wang,

Chengxiang Zhou,

Yifeng Han

et al.

Synthesis, Journal Year: 2024, Volume and Issue: unknown

Published: Oct. 21, 2024

Abstract Sulfonyl fluorides, due to their balanced potential reactivity and stability as well compatibility with biological systems, have become important synthetic intermediates building blocks in the fields of organic synthesis, drug discovery, materials science. Especially after report sulfur(VI) fluoride exchange (SuFEx) chemistry by Sharpless others, research on sulfonyl compounds related has increased significantly. This review summarizes application fluorides synthesis period 2014–2024, discussing different types reactions, including C–X bond formation (including C–C, C–N, C–F etc.), S–C formation, S–N S–O multicomponent ‘one-pot’ cyclization. 1 Introduction 2 Fluorides Applied (C, N, F) Bond Formation 3 4 5 6 Multicomponent Reactions 7 Cyclizations 8 Conclusion Perspective

Language: Английский

Nickel-catalyzed cross-electrophile couplings of aryl fluorosulfates with vinyl chlorosilanes DOI

Jin-He Na,

Hong-Jian Du,

Jia-Wen Jing

et al.

Journal of Catalysis, Journal Year: 2024, Volume and Issue: 437, P. 115636 - 115636

Published: July 6, 2024

Language: Английский

Citations

9

Influence of the Counterion on the Activation of Nickel(σ-Aryl) Precatalysts DOI Creative Commons

Ivo H. Lindenmaier,

Anna S. Harzer,

Markus Ströbele

et al.

Organometallics, Journal Year: 2025, Volume and Issue: unknown

Published: Feb. 2, 2025

Language: Английский

Citations

0

Nickel-Catalyzed Reductive Amidation of Aryl Fluorosulfates with Isocyanates: Synthesis of Amides via C–O Bond Cleavage DOI

Gan‐Qi Qin,

Jiao Wang,

Xu-Rong Cao

et al.

The Journal of Organic Chemistry, Journal Year: 2024, Volume and Issue: unknown

Published: Aug. 30, 2024

With the assistance of nickel as catalyst, 2,2'-bipyridine (bpy) ligand, and manganese reducing metal, reductive amidation isocyanates with readily accessible aryl fluorosulfates could be successfully accomplished. The reactions proceeded effectively via C-O bond activation in DMF at room temperature, enabling facile synthesis a range structurally diverse amides moderate to high yields broad functionality compatibility. In addition, synthetic usefulness method was further demonstrated by applying reaction scale-up late-stage functionalization complex molecules biological activities.

Language: Английский

Citations

3

The First Decade of SuFEx Chemistry: Advancements in SuFEx Polymerization, Non-Canonical SuFEx Reactions, and SuFEx Radiochemistry DOI

Min Pyeong Kim,

Manoj Kumar Sahoo, Joong‐Hyun Chun

et al.

Synthesis, Journal Year: 2024, Volume and Issue: unknown

Published: Oct. 7, 2024

Abstract This year marks the 10th anniversary of SuFEx chemistry, a field that has witnessed significant advancements over past decade. These include efficient synthetic strategies toward polymerization via approach leading to diverse polymers, alongside discovery new SuFExable hubs and coupling conditions. Non-canonical reactions, such as deoxyfluorination on-water have also emerged. Furthermore, there been substantial strides in radiosynthesis [18F] hubs. review provides an overview these developments, focusing on polymerization, non-canonical reaction, radiochemistry chemistry. 1 Introduction 2 Polymerization 3 Non-Canonical Reactions 4 Fluorine-18 Radiochemistry 5 Conclusions Outlook

Language: Английский

Citations

0

Application of Sulfonyl Fluorides in Organic Transformation DOI
Sichang Wang,

Chengxiang Zhou,

Yifeng Han

et al.

Synthesis, Journal Year: 2024, Volume and Issue: unknown

Published: Oct. 21, 2024

Abstract Sulfonyl fluorides, due to their balanced potential reactivity and stability as well compatibility with biological systems, have become important synthetic intermediates building blocks in the fields of organic synthesis, drug discovery, materials science. Especially after report sulfur(VI) fluoride exchange (SuFEx) chemistry by Sharpless others, research on sulfonyl compounds related has increased significantly. This review summarizes application fluorides synthesis period 2014–2024, discussing different types reactions, including C–X bond formation (including C–C, C–N, C–F etc.), S–C formation, S–N S–O multicomponent ‘one-pot’ cyclization. 1 Introduction 2 Fluorides Applied (C, N, F) Bond Formation 3 4 5 6 Multicomponent Reactions 7 Cyclizations 8 Conclusion Perspective

Language: Английский

Citations

0