Optimization of ZnO Nanoparticles’ Synthesis via Precipitation Method Applying Taguchi Robust Design DOI Open Access

Maria-Anna Gatou,

Katerina Kontoliou,

Eleni Volla

et al.

Catalysts, Journal Year: 2023, Volume and Issue: 13(10), P. 1367 - 1367

Published: Oct. 13, 2023

Zinc oxide (ZnO) possesses exceptional potential to be utilized in water and wastewater treatment applications, either as a photocatalyst or membrane incorporation. In the present study, ZnO nanoparticles were synthesized using precipitation method. The Taguchi approach with L32b orthogonal array was order optimize experimental conditions for synthesis of ensure that relatively smaller-sized particles obtained. design characterized by ten factors, where nine them possessed four levels, while one had two levels. This study’s factors type Zn precursor, concentration precipitating agent, agent’s concentration, solvent, pH value temperature used during synthetic procedure, calcination temperature, time stirring synthesis, well speed. influences those on selected response parameters (the average crystallite size, degree crystallinity, energy band gap (Eg), photodegradation constant (k)) then evaluated. XRD analysis calculated Eg values indicated hexagonal wurtzite structure only crystalline phase produced samples. photocatalytic efficiency all examined degradation rhodamine B under UV light irradiation. optimal achieved zinc acetate dihydrate precursor at equal 0.3 M, sodium hydroxide agent (1.5 M), methanol solvent 13), procedure 70 °C, 600 °C 90 min time, 700 rpm optimized sample based aforementioned thoroughly characterized. acquired results confirmed prediction approach, most enhanced k-value observed.

Language: Английский

Synergetic comparative study: Photocatalytic and biological investigations of green-synthesized metal oxide nanoparticles DOI

Rabiya Kousar,

Zia Ul Haq Khan, Sana Sabahat

et al.

Nano-Structures & Nano-Objects, Journal Year: 2024, Volume and Issue: 38, P. 101184 - 101184

Published: May 1, 2024

Language: Английский

Citations

4

A Review of Plant-Mediated ZnO Nanoparticles for Photodegradation and Antibacterial Applications DOI Creative Commons
Dorcas Mutukwa,

Raymond Tichaona Taziwa,

Lindiwe Khotseng

et al.

Nanomaterials, Journal Year: 2024, Volume and Issue: 14(14), P. 1182 - 1182

Published: July 11, 2024

This review focuses on the synthesis of plant-mediated zinc oxide nanoparticles (ZnO NPs) and their applications for antibacterial photocatalytic degradation dyes, thereby addressing need sustainable eco-friendly methods preparation NPs. Driven by significant rise in antibiotic resistance environmental pollution from dye pollution, there is a more effective agents photocatalysts. Therefore, this explores ZnO NPs, influence reaction parameters such as pH, annealing temperature, plant extract concentration, etc. Additionally, it also looks at application NPs photodegradation focusing properties size, shape, bandgap activity. The findings suggest that shape size are influenced these activity concludes have potential to advance green materials photocatalysis applications.

Language: Английский

Citations

4

Thiophene desulfurization: Effects of dendritic silica and PEG as surface modifier on ZnO photocatalyst DOI

Siti Nurfatin Nadhirah Mohd Makhtar,

Nur Hanis Hayati Hairom,

Nor Aliffah Puasa

et al.

Journal of Alloys and Compounds, Journal Year: 2024, Volume and Issue: 1003, P. 175703 - 175703

Published: July 24, 2024

Language: Английский

Citations

4

Development and evaluation of hydrogen peroxide mediated zinc oxide photocatalytic nanoparticles from Peepal (Ficus Religiosa) leaf extract for the treatment of actual tannery wastewater DOI

Ganeshkumar Govindasamy,

A. Babu Ponnusami

Environmental Science Water Research & Technology, Journal Year: 2025, Volume and Issue: unknown

Published: Jan. 1, 2025

Our findings offer insight into the impact of ZnO nanoparticles produced from Ficus Religiosa leaf extract on photocatalytic degradation tannery wastewater.

Language: Английский

Citations

0

Optimization of ZnO Nanoparticles’ Synthesis via Precipitation Method Applying Taguchi Robust Design DOI Open Access

Maria-Anna Gatou,

Katerina Kontoliou,

Eleni Volla

et al.

Catalysts, Journal Year: 2023, Volume and Issue: 13(10), P. 1367 - 1367

Published: Oct. 13, 2023

Zinc oxide (ZnO) possesses exceptional potential to be utilized in water and wastewater treatment applications, either as a photocatalyst or membrane incorporation. In the present study, ZnO nanoparticles were synthesized using precipitation method. The Taguchi approach with L32b orthogonal array was order optimize experimental conditions for synthesis of ensure that relatively smaller-sized particles obtained. design characterized by ten factors, where nine them possessed four levels, while one had two levels. This study’s factors type Zn precursor, concentration precipitating agent, agent’s concentration, solvent, pH value temperature used during synthetic procedure, calcination temperature, time stirring synthesis, well speed. influences those on selected response parameters (the average crystallite size, degree crystallinity, energy band gap (Eg), photodegradation constant (k)) then evaluated. XRD analysis calculated Eg values indicated hexagonal wurtzite structure only crystalline phase produced samples. photocatalytic efficiency all examined degradation rhodamine B under UV light irradiation. optimal achieved zinc acetate dihydrate precursor at equal 0.3 M, sodium hydroxide agent (1.5 M), methanol solvent 13), procedure 70 °C, 600 °C 90 min time, 700 rpm optimized sample based aforementioned thoroughly characterized. acquired results confirmed prediction approach, most enhanced k-value observed.

Language: Английский

Citations

10