Key Aspects in Designing High-Throughput Workflows in Electrocatalysis Research: A Case Study on IrCo Mixed-Metal Oxides DOI Creative Commons
Joanna Magdalena Przybysz, Ken J. Jenewein, Mária Minichová

et al.

ACS Materials Letters, Journal Year: 2024, Volume and Issue: 6(11), P. 5103 - 5111

Published: Oct. 15, 2024

With the growing interest of electrochemical community in high-throughput (HT) experimentation as a powerful tool accelerating materials discovery, implementation HT methodologies and design workflows has gained traction. We identify 6 aspects essential to workflow electrochemistry beyond ease incorporation methods community's research assist their improvement. study IrCo mixed-metal oxides (MMOs) for oxygen evolution reaction (OER) acidic media using mentioned provide practical example possible pitfalls strategies counteract them.

Language: Английский

Self-Driving Laboratories for Chemistry and Materials Science DOI Creative Commons
Gary Tom, Stefan P. Schmid, Sterling G. Baird

et al.

Chemical Reviews, Journal Year: 2024, Volume and Issue: 124(16), P. 9633 - 9732

Published: Aug. 13, 2024

Self-driving laboratories (SDLs) promise an accelerated application of the scientific method. Through automation experimental workflows, along with autonomous planning, SDLs hold potential to greatly accelerate research in chemistry and materials discovery. This review provides in-depth analysis state-of-the-art SDL technology, its applications across various disciplines, implications for industry. additionally overview enabling technologies SDLs, including their hardware, software, integration laboratory infrastructure. Most importantly, this explores diverse range domains where have made significant contributions, from drug discovery science genomics chemistry. We provide a comprehensive existing real-world examples different levels automation, challenges limitations associated each domain.

Language: Английский

Citations

39

Autonomous chemistry: Navigating self-driving labs in chemical and material sciences DOI

Oliver Bayley,

Elia Savino,

Aidan Slattery

et al.

Matter, Journal Year: 2024, Volume and Issue: 7(7), P. 2382 - 2398

Published: July 1, 2024

Language: Английский

Citations

9

Artificial Intelligence Meets Laboratory Automation in Discovery and Synthesis of Metal–Organic Frameworks: A Review DOI
Yiming Zhao,

Yongjia Zhao,

Jian Wang

et al.

Industrial & Engineering Chemistry Research, Journal Year: 2025, Volume and Issue: 64(9), P. 4637 - 4668

Published: Feb. 24, 2025

This review discusses the transformative impact of convergence artificial intelligence (AI) and laboratory automation on discovery synthesis metal–organic frameworks (MOFs). MOFs, known for their tunable structures extensive applications in fields such as energy storage, drug delivery, environmental remediation, pose significant challenges due to complex processes high structural diversity. Laboratory has streamlined repetitive tasks, enabled high-throughput screening reaction conditions, accelerated optimization protocols. The integration AI, particularly Transformers large language models (LLMs), further revolutionized MOF research by analyzing massive data sets, predicting material properties, guiding experimental design. emergence self-driving laboratories (SDLs), where AI-driven decision-making is coupled with automated experimentation, represents next frontier research. While remain fully realizing potential this synergistic approach, AI heralds a new era efficiency innovation engineering materials.

Language: Английский

Citations

1

Autonomous laboratories for accelerated materials discovery: a community survey and practical insights DOI Creative Commons
Linda Hung,

Joyce A. Yager,

Danielle R. Monteverde

et al.

Digital Discovery, Journal Year: 2024, Volume and Issue: 3(7), P. 1273 - 1279

Published: Jan. 1, 2024

We share the results of a survey on automation and autonomy in materials science labs, which highlight variety researcher challenges motivations. also propose framework for levels laboratory from L0 to L5.

Language: Английский

Citations

4

Automation and Machine Learning for Accelerated Polymer Characterization and Development: Past, Potential, and a Path Forward DOI
Peter A. Beaucage, Duncan R. Sutherland, Tyler B. Martin

et al.

Macromolecules, Journal Year: 2024, Volume and Issue: unknown

Published: Sept. 7, 2024

Language: Английский

Citations

4

Archerfish: a retrofitted 3D printer for high-throughput combinatorial experimentation via continuous printing DOI Creative Commons
Alexander E. Siemenn, Basita Das, Eunice Aissi

et al.

Digital Discovery, Journal Year: 2025, Volume and Issue: unknown

Published: Jan. 1, 2025

Archerfish is a low-cost, high-throughput tool for combinatorial materials research. Retrofitted with in situ mixing, prints 250 unique compositions per min—a 100× acceleration factor—for aqueous, nanoparticle, and crystalline materials.

Language: Английский

Citations

0

Solvent Screening for Separation Processes Using Machine Learning and High-Throughput Technologies DOI Creative Commons

Justin P. Edaugal,

Difan Zhang, Dupeng Liu

et al.

Chem & Bio Engineering, Journal Year: 2025, Volume and Issue: 2(4), P. 210 - 228

Published: March 5, 2025

As the chemical industry shifts toward sustainable practices, there is a growing initiative to replace conventional fossil-derived solvents with environmentally friendly alternatives such as ionic liquids (ILs) and deep eutectic (DESs). Artificial intelligence (AI) plays key role in discovery design of novel development green processes. This review explores latest advancements AI-assisted solvent screening specific focus on machine learning (ML) models for physicochemical property prediction separation process design. Additionally, this paper highlights recent progress automated high-throughput (HT) platforms screening. Finally, discusses challenges prospects ML-driven HT strategies optimization. To end, provides insights advance future

Language: Английский

Citations

0

Science acceleration and accessibility with self-driving labs DOI Creative Commons
Richard B. Canty, Jeffrey A. Bennett, Keith A. Brown

et al.

Nature Communications, Journal Year: 2025, Volume and Issue: 16(1)

Published: April 24, 2025

Language: Английский

Citations

0

The evolving role of programming and LLMs in the development of self-driving laboratories DOI Creative Commons
John R. Kitchin

APL Machine Learning, Journal Year: 2025, Volume and Issue: 3(2)

Published: April 30, 2025

Machine learning and automation are transforming scientific research, yet the implementation of self-driving laboratories (SDLs) remains costly complex, it difficult to learn how use these facilities. To address this, we introduce Claude-Light, a lightweight, remotely accessible instrument designed for prototyping algorithms machine workflows. Claude-Light integrates REST API, Raspberry Pi-based control system, an RGB LED with photometer that measures ten spectral outputs, providing controlled but realistic experimental environment. This device enables users explore at multiple levels, from basic programming design learning-driven optimization. We demonstrate application in structured approaches, including traditional scripting, statistical experiments, active methods. In addition, role large language models (LLMs) laboratory automation, highlighting their selection, data extraction, function calling, code generation. While LLMs present new opportunities streamlining they also challenges related reproducibility, security, reliability. discuss strategies mitigate risks while leveraging enhanced efficiency laboratories. provides practical platform students researchers develop skills test before deploying them larger-scale SDLs. By lowering barrier entry this tool facilitates broader adoption AI-driven experimentation fosters innovation autonomous

Language: Английский

Citations

0

The Implementation and Impact of Chemical High-Throughput Experimentation at AstraZeneca DOI
James J. Douglas, Andrew D. Campbell, David Buttar

et al.

ACS Catalysis, Journal Year: 2025, Volume and Issue: unknown, P. 5229 - 5256

Published: March 13, 2025

Language: Английский

Citations

0