Advancements in solvent microextraction: Recent developments and diverse applications in the modern era DOI
Priyanka Rani, Bibhu Prasad Nanda, Raj Kumar Narang

et al.

Separation Science Plus, Journal Year: 2024, Volume and Issue: 7(6)

Published: March 3, 2024

Abstract Solvent microextraction (SME) is designed to selectively isolate desired analytes while minimizing the presence of interfering substances in extracted sample. There are different approaches from which single‐drop (SDME) can be amalgamated with various analytical methods enhance its functionalities and improve analysis compounds like gas chromatography, liquid chromatography amplify sensitivity, selectivity, capacity detect trace amounts complex matrices. The review focuses on intricacies solid‐phase elucidates operational principles. Additionally, it explores types SDMEs, detailing their respective benefits, drawbacks, potential applications future. A typical explanation construction working hollow fiber‐liquid phase as well has been discussed. SMEs medical biomedical fields food environmental purification water, organic pollutants, drug analysis, screening new drugs have discussed also illustrated tabular form. pros cons both techniques given a manner broad comparison between advanced SME provides direction for monitoring, safety, refining impurities water samples. comprehensive overview current progress, recent obstacles, future possibilities an appropriate manner. Despite numerous promising advancements, utilization remains challenging field.

Language: Английский

Solid phase microextraction for the bioanalysis of emerging organic pollutants DOI

Xiaoying Feng,

Yixin Kuang,

L.‐S. Gan

et al.

TrAC Trends in Analytical Chemistry, Journal Year: 2024, Volume and Issue: 177, P. 117786 - 117786

Published: May 22, 2024

Language: Английский

Citations

14
Skin emitted volatiles analysis for noninvasive diagnosis: the current advances in sample preparation techniques for biomedical application DOI Creative Commons

S. Keerthana,

Mohammad Saquib,

Harshika Poojary

et al.

RSC Advances, Journal Year: 2024, Volume and Issue: 14(17), P. 12009 - 12020

Published: Jan. 1, 2024

Human skin emits a series of volatile compounds from the due to various metabolic processes, microbial activity, and several external factors. Changes in concentration metabolites indicate many diseases, including diabetes, cancer, infectious diseases. Researchers focused on skin-emitted gain insight into pathophysiology In case volatolomics research, it is noteworthy that sample preparation, sampling protocol, analytical techniques, comprehensive validation are important for successful integration profiles regular clinical settings. Solid-phase microextraction techniques polymer-based active sorbent traps were developed capture compounds. The primary advantage these preparation ability efficiently targetedly metabolites, thus improving detection biomarkers associated with further polydimethyl-based patches utilized research their biocompatibility thermal stability properties. tools coupled high sensitive Gas Chromatography-Mass Spectrometer provided potential platform volatolomes, emerging as state-of-the-art technique. Later, technological advancements, design wearable sensors, have enriched skin-based can integrate information portable platform. However, individual-specific hydration, temperature, conditions influence variations concentration. Considering subject-specific depth, time standardization, suitable may improve discovery marker Here, we summarised current progress, limitations, advances disease diagnosis, monitoring, personalized healthcare applications.

Language: Английский

Citations

11
Applications of magnetic solid‐phase extraction in the sample preparation of natural product analysis (2020–2023) DOI
Lingxiao Chen, Feng Yang

Journal of Separation Science, Journal Year: 2024, Volume and Issue: 47(11)

Published: May 31, 2024

Sample preparation, including extraction, separation, and purification, is a vital process for natural product analysis. As an attractive sample pretreatment method, magnetic solid‐phase extraction (MSPE) has gained plenty of attention, mainly due to its simpler operation, less consumption organic solvents, shorter processing time than traditional SPE. This updated review devoted summarizing the applications MSPE based on different nanomaterials in analysis various products complex matrixes, such as biological samples, plants, Chinese herbal preparations past four years (2020–2023). The preparation fabrication materials are briefly introduced. Furthermore, mechanism interaction forces between adsorbent analytes elaborated, advantages disadvantages adsorbents coupled with analytical methods summarized. Moreover, future trends opportunities discussed. It expected that this work can provide information research fields.

Language: Английский

Citations

11
Nanoscale-controlled organic inorganic hybrid spheres for comprehensive enrichment of ultratrace chlorobenzenes in marine and fresh water DOI

Yixin Kuang,

Suxin Zhou,

Yuefan Liu

et al.

Journal of Hazardous Materials, Journal Year: 2024, Volume and Issue: 466, P. 133541 - 133541

Published: Jan. 18, 2024

Language: Английский

Citations

10
Development of a high-efficiency and environmentally friendly melamine–formaldehyde resin-based solid phase microextraction fiber for enhanced extraction of polycyclic aromatic hydrocarbons from environmental water DOI
Peng-Fei Li,

Yehong Han,

Dandan Han

et al.

Green Chemistry, Journal Year: 2024, Volume and Issue: 26(6), P. 3211 - 3220

Published: Jan. 1, 2024

A new eco-friendly method was developed to synthesize rough surface, uniform particle size, and high heat-resistant fiber coating materials in water medium, achieving a remarkable enrichment capacity for trace pollutants environmental water.

Language: Английский

Citations

10
Porous chlorine-functionalized covalent organic framework anchored graphene aerogel composite for synergically enhanced solid phase microextraction of polychlorinated naphthalene in environmental water DOI

Lansen Yang,

Pengfei Li,

Yehong Han

et al.

Journal of Hazardous Materials, Journal Year: 2024, Volume and Issue: 469, P. 133909 - 133909

Published: Feb. 27, 2024

Language: Английский

Citations

10
Monitoring Poly(methyl methacrylate) and Polyvinyl Dichloride Micro/Nanoplastics in Water by Direct Solid-Phase Microextraction Coupled to Gas Chromatography–Mass Spectrometry DOI
Shengrui Xu, Huimin Li, Xiao Li

et al.

Analytical Chemistry, Journal Year: 2024, Volume and Issue: 96(26), P. 10772 - 10779

Published: June 21, 2024

A simple, sustainable, and sensitive monitoring approach of micro/nanoplastics (MNPs) in aqueous samples is crucial since it helps assessing the extent contamination understanding potential risks associated with their presence without causing additional stress to environment. In this study, a novel strategy for qualitative quantitative determination MNPs water by direct solid-phase microextraction (SPME) coupled gas chromatography–mass spectrometry (GC-MS) was proposed first time. Spherical poly(methyl methacrylate) (PMMA) irregularly shaped polyvinyl dichloride (PVDC) were used evaluate feasibility performance method. The results demonstrated that both PMMA PVDC efficiently extracted homemade SPME coating nitrogen-doped porous carbons (N-SPCs) exhibited sufficient thermal decomposition GC-MS injection port. Excellent extraction performances N-SPCs are attributed hydrophobic cross-linking, electrostatic forcing, hydrogen bonding, pore trapping. Methyl methacrylate identified as marker PMMA, while 1,3-dichlorobenzene 1,3,5-trichlorobenzene indicators PVDC. Under optimal conditions, method ultrahigh sensitivity, limit detection 0.0041 μg/L 0.0054 Notably, programmed temperature injector developed discriminate eliminate interferences intrinsic indicator compounds. Owing integration sampling, extraction, injection, into one step SPME, demonstrates exceptional eliminating necessity complex sample pretreatment procedures use organic solvents. Finally, successfully applied real samples.

Language: Английский

Citations

10
Defective porous urchin-like ZnO/NiO microspheres-coated solid-phase microextraction fiber for analysis of trace polychlorinated biphenyls in milk DOI
Shiping Zhu,

Zhen Song,

Youmei Wang

et al.

Journal of Hazardous Materials, Journal Year: 2024, Volume and Issue: 480, P. 136362 - 136362

Published: Oct. 31, 2024

Language: Английский

Citations

9
Monolithic metal–organic framework-808 fiber as a novel coating for headspace solid-phase microextraction of phthalate esters from PET containers using GC–MS DOI

Hanieh Kefayati,

Yadollah Yamini,

Seyedeh Sara Nasrollahi

et al.

Microchemical Journal, Journal Year: 2025, Volume and Issue: 209, P. 112645 - 112645

Published: Jan. 2, 2025

Language: Английский

Citations

1
Microextraction-Based Techniques for the Determination of Beta-Blockers in Biological Fluids: A Review DOI Creative Commons

Styliani Nisyriou,

Constantinos K. Zacharis

Separations, Journal Year: 2025, Volume and Issue: 12(1), P. 14 - 14

Published: Jan. 12, 2025

Sample preparation is a critical step in the analytical process. Apart from traditional sample cleanup approaches, microextraction-based techniques have attracted much attention recent years and especially researchers working analysis of beta-blockers. Developing sensitive selective methods essential for detecting these compounds complex matrices. The present review aims to provide an overview determination beta-blockers biological samples, covering time frame last decade. Detailed information on materials/coatings instrumental configurations are provided.

Language: Английский

Citations

1