Improvement of cocoa powder properties through ultrasonic- and microwave-assisted alkalization DOI Creative Commons

Dimas Rahadian Aji Muhammad,

Dhavid Ramadhan Pratama,

Danar Praseptiangga

et al.

Open Agriculture, Journal Year: 2024, Volume and Issue: 9(1)

Published: Jan. 1, 2024

Abstract Improving the process efficiency is still a challenge in alkalization of cocoa powder. This research aims to study effect ultrasonic- and microwave-assisted on quality attributes Three levels duration were used (5, 10, 15 min), then physical antioxidant properties powder evaluated. The results show that more effective improving powder’s darkness red intensity than conventional process. produced using significantly improved pH 7.59, solubility from 20 28% wetting time almost twice, depending type However, both advanced methods caused significant decrease total phenols, flavonoids, activity by about 35, 22, 38%, respectively, compared method. provides further information potential use ultrasonication microwave techniques, particularly processing has not been explored previously.

Language: Английский

Profile of Bioactive Components of Cocoa (Theobroma cacao L.) By-Products from Ecuador and Evaluation of Their Antioxidant Activity DOI Creative Commons
Wilma Llerena, Iván Samaniego, Christian Vallejo

et al.

Foods, Journal Year: 2023, Volume and Issue: 12(13), P. 2583 - 2583

Published: July 3, 2023

The aim of the study was to determine profile bioactive compounds in cocoa residues (mucilage and bean shells), evaluate their antioxidant activity two varieties, Nacional X Trinitario type (Fine Aroma) variety CCN-51. extraction phytonutrients from carried out selectively. characterization quantification total polyphenol content (TPC), flavonoid (TFC) were determined by UV-VIS spectrophotometry. High-performance liquid chromatography (HPLC) used phenolic methylxanthines. evaluated methods 2-azinobis (3-ethyl-benzothiazoline-6-sulfonic acid) cation bleaching (ABTS), ferric-reducing power (FRAP) oxygen radical absorbance capacity (ORAC). exudate mucilage samples Trinitario-type presented highest TPC 105.08 mg gallic acid equivalents (GAE)/100 mL, TFC 36.80 catechin (CE)/100 (CAT) 35.44 mg/g, procyanidins (PCB2: 35.10; PCB1: 25.68; PCC1: 16.83 mg/L), epicatechin (EPI) 13.71 mg/L, caffeine (CAF) 0.90% theobromine (TBR) 2.65%. In shell, CCN-51 a higher (42.17 GAE/100 g) (20.57 CE/100 g). However, CAT (16.16 mg/g), CAF (0.35%) TBR (1.28%) type. EPI no significant differences between studied (0.83 0.84 mg/g). values (ABTS, FRAP ORAC methods) than shell 171.32, 192.22 56.87 Trolox (TE)/g, respectively, 167.06, 160.06 52.53 TE/g, respectively. ORAC) correlated with shells, showing strong positive correlation (<0.99) (B1, B2 C1), positive/moderate (0.94)

Language: Английский

Citations

17

Combined effect of pulse electric field and probe ultrasound technologies for obtaining phenolic compounds from orange by-product DOI Creative Commons
María del Carmen Razola‐Díaz, Robert Sevenich, Luma Rossi Ribeiro

et al.

LWT, Journal Year: 2024, Volume and Issue: 198, P. 115950 - 115950

Published: March 11, 2024

Orange peel by-product is a known source of bioactive compounds with several health benefits. This study focuses on optimizing the conditions for pulsed electric field (PEF) technology as pretreatment to obtain extracts rich in phenolic from orange peel. A Box-Behnken design 15 experiments 3 independent factors (field energy, number pulses and pulse width) was performed. The content extracted by ultrasound analyzed HPLC-ESI-TOF-MS. Optimum were 1.4 kV/cm 30 110 μs achieving recovery 40.8 mg/g dry weight compounds, 27.5% higher than obtained without PEF. Besides, hesperidin narirutin increased 29.4 38.9%, respectively. For antioxidant assays also significative increments (≥53%) achieved. combination optimized PEF pre-treatment extraction has let enriched polyphenols activity.

Language: Английский

Citations

8

Comparative evaluation of the physicochemical properties and prebiotic potential of cocoa (Theobroma cacao L.) bean shell and commercial cocoa powders with varying degrees of alkalization DOI Creative Commons

Aiza B. Umali,

Argel A. Largado,

John Joseph C. Menia

et al.

Discover Food, Journal Year: 2025, Volume and Issue: 5(1)

Published: March 27, 2025

Language: Английский

Citations

0

Diet enriched with high-phenolic cocoa potentiates hippocampal brain-derived neurotrophic factor expression and neurogenesis in healthy adult micewith subtle effects on memory DOI Creative Commons
Sonia Melgar‐Locatelli, M. Carmen Mañas‐Padilla, Adriana Castro‐Zavala

et al.

Food & Function, Journal Year: 2024, Volume and Issue: 15(16), P. 8310 - 8329

Published: Jan. 1, 2024

Cocoa is widely known for its health benefits, but neurocognitive impact remains underexplored. This preclinical study aimed to investigate the effects of cocoa and polyphenols on hippocampal neuroplasticity, cognitive function emotional behavior. Seventy young-adult C57BL/6JRj male female mice were fed either a standard diet (CTR) or enriched with 10% high-phenolic content (HPC) low-phenolic (LPC) at least four weeks. In first experiment, behavioral tests assessing exploratory behavior, responses hippocampal-dependent memory conducted weeks into diet, followed by animal sacrifice week later. Adult neurogenesis brain-derived neurotrophic factor (BDNF) expression in hippocampus prefrontal cortex evaluated using immunohistochemistry western blot. different synaptic response, long-term potentiation presynaptic-dependent short-term plasticity studied electrophysiology. Cocoa-enriched diets had minimal activity anxiety-like except reduced locomotion LPC group. Only HPC enhanced object recognition memory, while place spatial navigation remained unaffected. The also increased adult neurogenesis, boosting proliferation, survival number young adult-born neurons. However, both cocoa-enriched immobility forced swimming test BDNF expression. Hippocampal electrophysiology revealed no alterations neuroplasticity among diets. results mostly unaffected sex. Overall, demonstrated greater potential regarding neuroplastic suggesting key role flavanols dietary interventions enhancing brain health.

Language: Английский

Citations

3

Factors affecting consumer perception and acceptability of chocolate beverages DOI Creative Commons
Marta Palma‐Morales, Christina J. Birke Rune, Estela Castilla‐Ortega

et al.

LWT, Journal Year: 2024, Volume and Issue: 201, P. 116257 - 116257

Published: May 27, 2024

The factors influencing consumer acceptability of hot cocoa-based beverages prepared with pure cocoa powders were studied. Five samples originating from various regions selected, including both alkalized and non-alkalized (natural) powders, regular fat-reduced powders. Sensory evaluation the was conducted using a 5-point just-about-right (JAR) scale 9-point hedonic scale, total 116 participants involved in study. Principal Component Analysis (PCA) highlighted relationship between alkalization, fat content, phenolic composition. Alkalized received higher scores than natural ones color (6.9 vs 5.6), smell (5.9 5.7), flavor (5.8 4.9), texture (6.0 5.7) overall 5.2), all categories, while low-fat evaluated less favorably powder (6.6 5.8), (6.3 5.4), 4.8), (6.2 5.6) (6.1 5.1). Additionally, A content above 30 g GAE/kg d.w. resulted decreased preference. Comprehensive insights on effect reduction alkalization process physicochemical sensory properties are provided, contributing to intricate array products. It is important note that origin may also influence composition, underscoring need for further studies explore this variable.

Language: Английский

Citations

2

A Survey on Potentially Beneficial and Hazardous Bioactive Compounds in Cocoa Powders Samples Sourced from European Market DOI Open Access
Luigi Esposito, Matteo Perillo, Carla Di Mattia

et al.

Published: July 1, 2024

Cocoa (Theobroma Cacao, L.) represents an important market that gained relevance and became esteemed commodity thanks to cocoa powder, chocolate, other related products. This work has analyzed 59 powder samples from the European market. Three distinct subgroups were identified: organic or conventional, alkalized not alkalized, raw roasted processing. The impact of technological process was evaluated on pH, color, compositional traits, as content biogenic amines salsolinol. phenolic fraction also investigated trough both common emerging methods. Results depict influence agronomical practices (organic/conventional) did affect significatively (p&amp;lt;0.05) composition powders; similarly, roasting discriminative for compounds traced. On hand, alkalinization greatly impacted no matter provenience, obtention, processes, resulting reducing treated samples. Principal components analysis confirmed alkali acts composition, but bioactives molecules (BAs salsolinol). All resulted safe while powders have a great reduction in beneficial biocompounds. A novel strategy could be emphasize non-alkalized label, meet demand more

Language: Английский

Citations

2

Integration of network-based approaches for assessing variations in metabolic profiles of alkalized and non-alkalized commercial cocoa powders DOI Creative Commons
Marta Palma‐Morales, Óscar Daniel Rangel-Huerta,

Caridad Díaz

et al.

Food Chemistry X, Journal Year: 2024, Volume and Issue: 23, P. 101651 - 101651

Published: July 16, 2024

Cocoa can undergo an alkalization process to enhance its color and solubility. It reduces astringency alters composition, particularly in the phenolic compound content, which is related cocoa health benefits. This study aimed investigate impact of on composition seven commercial powders. A liquid chromatography-based metabolomic approach was employed assess metabolic differences between alkalized non-alkalized Supervised orthogonal partial least squares discriminant analysis (OPLS-DA) used identify most discriminating variables groups. feature-based molecular network (FBMN) explore chemical space. Three hundred forty-seven metabolites were obtained as discriminant, among 60 tentatively annotated. Phenolic compounds, lysophosphatidylethanolamines, amino acids, their derivatives significantly reduced cocoas. In contrast, fatty acids increased with alkalization. Despite variability cocoas, chemometrics allowed elucidation alterations induced specifically by composition.

Language: Английский

Citations

2

Impact of cocoa variety on physical and chemical properties, reconstitutability, and flowability of cocoa powders DOI
Surprise Moussoyi Moundanga, Jérémy Petit,

C. B. Ndangui

et al.

Powder Technology, Journal Year: 2024, Volume and Issue: 447, P. 120214 - 120214

Published: Aug. 24, 2024

Language: Английский

Citations

2

Response Surface Methodology for the Optimization of Flavan-3-ols Extraction from Avocado By-Products via Sonotrode Ultrasound-Assisted Extraction DOI Creative Commons
María del Carmen Razola‐Díaz, Vito Verardo, Eduardo Guerra‐Hernández

et al.

Antioxidants, Journal Year: 2023, Volume and Issue: 12(7), P. 1409 - 1409

Published: July 11, 2023

Avocado peel and seed are the main by-products of avocado processing considered as promising sources phenolic compounds with biological activities. Thus, this research focuses on establishment, for first time, ultrasound-assisted extraction flavan-3-ols high antioxidant activity from using a sonotrode. Indeed, 2 Box-Behnken designs were performed 15 experiments, each design having three independent factors (ratio ethanol/water (v/v), time (min) amplitude (%)). In both models, responses included total procyanidins (flavan-3-ols) measured via HPLC-FLD DPPH, ABTS FRAP. The results showed that applying sonotrode method could increase recovery by 54% 62-76% compared to ultrasound bath technology. Therefore, technology was demonstrated be non-thermal, low time-consuming scalable allowed used functional ingredients.

Language: Английский

Citations

6

Enhanced extraction of procyanidins from avocado processing residues by pulsed electric fields pre-treatment. DOI Creative Commons
María del Carmen Razola‐Díaz, Jessica Genovese, Urszula Tylewicz

et al.

LWT, Journal Year: 2024, Volume and Issue: 212, P. 116952 - 116952

Published: Oct. 25, 2024

Language: Английский

Citations

2